A high temperature resistant low ablation coating and its preparation method
A technology of high temperature resistance and coating, applied in the field of surface engineering, can solve the problems of high preparation cost, complicated process, difficult to widely apply coating system, etc., and achieve the effect of good effect and simple preparation process.
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Embodiment 1
[0029] Firstly, the anti-oxidation transition layer was prepared by spraying 5wt% perhydrosilazane on the composite material substrate, and brushed 3 times with an interval of 10 minutes between 2 times.
[0030]Next, prepare the heat-absorbing low-ablative layer slurry, and its raw material ratio is: polysiloxazane 35wt%, zirconia fiber 25wt%, carbon fiber 5wt%, hafnium carbide 30wt%, phenolic resin ball 5wt%, adopt brush coating Process The coating was prepared with a coating thickness of 3 mm, and then cured at room temperature for 12 hours.
[0031] Finally, a low-ablation radiation heat dissipation surface layer slurry was prepared, the raw material ratio of which was: polysiloxazane 40wt%, hafnium carbide 60wt%, using a brushing process, the coating thickness was 0.5mm, and then cured at room temperature for 12 hours.
[0032] The high-temperature-resistant and low-ablation coating is ablated by plasma flame at 2000°C for 100s, and the maximum temperature of the carbon-c...
Embodiment 2
[0034] Firstly, the anti-oxidation transition layer was prepared by spraying 15wt% perhydrosilazane on the composite material substrate, and brushed for 3 times with an interval of 15 minutes between 2 times.
[0035] Next, prepare the heat-absorbing low-ablative layer slurry, its raw material ratio is: polysiloxazane 25wt%, zirconia fiber 35wt%, carbon fiber 8wt%, hafnium boride 30wt%, phenolic resin ball 2wt%, adopt spraying Process The coating was prepared with a coating thickness of 0.3 mm, and then cured at room temperature for 24 hours.
[0036] Finally, a low-ablation radiation heat dissipation surface layer slurry is prepared, the raw material ratio of which is: polysiloxazane 20wt%, hafnium boride 80wt%, spraying process, coating thickness 0.5mm, and then curing at room temperature for 24 hours.
[0037] The high-temperature-resistant and low-ablation coating is ablated by plasma flame at 2000°C for 100s, and the maximum temperature of the carbon-carbon substrate is 5...
Embodiment 3
[0039] Firstly, the anti-oxidation transition layer was prepared by spraying 25wt% perhydrosilazane on the composite material substrate, and brushed 3 times with an interval of 20 minutes between 2 times.
[0040] Secondly, prepare the heat-absorbing low-ablative layer slurry, the raw material ratio is: polysiloxazane 30wt%, zirconia fiber 25wt%, carbon fiber 5wt%, zirconium carbide 35wt%, phenolic resin ball 5wt%, using a spraying process The coating was prepared with a coating thickness of 2 mm, and then cured at room temperature for 18 hours.
[0041] Finally, a low-ablation radiation heat dissipation surface layer slurry was prepared. The raw material ratio was: polysiloxazane 30wt%, hafnium oxide 70wt%, spraying process, coating thickness 0.05mm, and then curing at room temperature for 18 hours.
[0042] The high-temperature-resistant and low-ablation coating is ablated by plasma flame at 2000°C for 100s, and the maximum temperature of the carbon-carbon substrate is 360°C...
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