A method for preparing functional oil and active protein powder from hollyhock
A functional technology of hollyhock, which is applied in the processing field of hollyhock, can solve the problems of cumbersome refining process, long time consumption, bad protein denaturation in the cake, etc., and achieve the effect of short process flow and high efficiency
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Embodiment 1
[0047] 1 Raw material treatment: remove impurities, wash and drain fresh hollyhock seeds, dry them with low-temperature blast for about 25 hours, so that the water content reaches about 6%, shell them by conventional techniques, compact them, weigh them, and put them into a subcritical extraction kettle.
[0048] 2. Subcritical extraction
[0049] Compress the subcritical extractant (alkane) into a liquid state at a temperature of <35°C and a pressure of 0.5Mpa, inject it into the extraction kettle, stir and mix with the seed blank, and keep the volume ratio of the extraction solvent to the seed blank greater than 2:1, and control Solvent temperature < 35°C, system pressure 0.6MPa, extraction time 50min, filter to separate the solid and liquid phases, transfer the liquid phase mixed solution into a temporary storage tank, and complete a immersion extraction.
[0050] 3. Analysis
[0051] After soaking and extracting for 3-4 times, the mixed solution in the temporary storage t...
Embodiment 2
[0061] 1. Raw material processing: remove impurities, wash and drain fresh hollyhock seeds, dry them with low-temperature blast for about 26 hours, and make the water content reach about 5%. After conventional dehulling, compaction, weighing, put them into a subcritical extraction kettle.
[0062] 2. Subcritical extraction
[0063] Compress the subcritical extractant (alkane) into a liquid state at a temperature of <40°C and a pressure of 0.6MPa, inject it into the extraction kettle, stir and mix with the seed body, and keep the volume ratio of the extraction solvent to the seed body greater than 3:1, and control Solvent temperature < 40°C, system pressure 0.6MPa, extraction time 60min, filter to separate the solid and liquid phases, transfer the liquid phase mixed solution into a temporary storage tank, and complete a immersion extraction.
[0064] 3. Analysis
[0065] After soaking and extracting for many times, the mixed solution in the temporary storage tank is transporte...
Embodiment 3
[0075] 1. Raw material treatment: remove impurities, wash and drain fresh hollyhock seeds, dry them with low-temperature blast for about 26 hours, and use a water content of about 4%. After conventional husking, compaction, weighing, put them into a subcritical extraction kettle.
[0076] 2. Subcritical extraction
[0077] Compress the subcritical extractant (alkane) into a liquid state at a temperature <45°C and a pressure of 0.7mpa, inject it into the extraction kettle, stir and mix with the seed body, and keep the volume ratio of the extraction solvent to the seed body greater than 4:1, and control The solvent temperature is <45°C, the system pressure is 0.7MPa, and the extraction time is 70 minutes. The solid and liquid phases are separated by filtration, and the liquid phase mixed solution is transported into a temporary storage tank to complete a soaking extraction.
[0078] 3. Analysis
[0079] After soaking and extracting for many times, the mixed solution in the temp...
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