Preparation method of antifogging and antireflection film coating liquid
A technology of anti-reflection film and manufacturing method, which is applied in the direction of coating, etc., can solve the problems of glass surface clarity reduction, refractive index change, etc., achieve good optical performance, improve flexibility, and meet the effects of high-speed production
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Embodiment 1
[0056] (1) Disperse 4.625Kg of nano-silica with a particle size of 5nm in 87.875Kg of deionized water to prepare a dispersion with a concentration of 5%. Add 2.775Kg of ethanol to the dispersion to prepare a concentration of 5% by mass 3-(Methacryloyloxy)propyltrimethoxysilane solution, heated to 70°C under stirring, and kept at this temperature for 30 minutes;
[0057] (2) Add 2.9193Kg ethanol, 23.7513Kg deionized water, 1.190Kg acrylic acid, 0.158Kg methacrylic acid, 0.06625Kg ethylene glycol dimethacrylate dropwise to the solution of step (1) under stirring Mix the solution, stir and mix at 70°C for 40 minutes, then add 0.09225Kg potassium persulfate, react in a sealed reaction device for 8 hours, and obtain a core-shell structure spherical acrylic acid and difunctional methacrylate copolymer with a particle size of 35nm after cooling -Silicon dioxide colloidal nanocomposite light blue dispersion;
[0058] (3) Dilute the nanocomposite dispersion in step (2) with a deionize...
Embodiment 2
[0062] Change the consumption ratio of acrylic acid and methacrylic acid, add 1.058Kg acrylic acid, 0.315Kg methacrylic acid, repeat the manufacturing method of embodiment 1.
[0063] The performance test data of the obtained anti-fog and anti-reflection film are shown in Table 1.
Embodiment 3
[0065] Change the consumption ratio of acrylic acid and methacrylic acid, add 0.925Kg acrylic acid, 0.473Kg methacrylic acid, repeat the manufacturing method of embodiment 1.
[0066] The performance test data of the obtained anti-fog and anti-reflection film are shown in Table 1.
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