Ceramic separator with high inorganic solid content and its application in lithium-ion battery system
A technology of ceramic diaphragm and solid phase content, applied in battery pack parts, circuits, electrical components, etc., can solve problems such as potential safety hazards, and achieve the effects of strong puncture resistance, not easy to break, and good process controllability
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Embodiment 1
[0028] Example 1: Aluminum oxide fiber membrane S1
[0029] Dissolve 2.0g of aluminum nitrate in 20g of deionized water, then add 20g of polyvinyl alcohol solution with a mass concentration of 10%, and stir thoroughly to obtain a precursor solution; add the precursor solution into the syringe of the electrospinning equipment, and spin The method is to obtain precursor fibers (spinning conditions: spinning voltage 30KV, extrusion speed 2.0ml / min); repeat the above process several times to obtain multiple precursor fibers; remove all the fibers from the receiving plate, and place them in a medium temperature furnace Calcined at 1000° C. for 10 hours, collected 50.5 g of aluminum oxide fiber powder in total; the average length of the obtained aluminum oxide fibers was 0.5 μm, and the average diameter was 0.05 μm. Soak the aluminum oxide fiber powder in a silane coupling agent solution, filter, and dry to carry out surface lipophilic modification treatment; weigh 25.0 g of the pre...
Embodiment 2
[0030] Example 2: Zirconia fiber membrane S2
[0031] Dissolve 2.0g of zirconium oxynitrate in 20g of deionized water, then add 20g of 10% polyvinyl alcohol solution in mass concentration, and stir thoroughly to obtain a precursor solution; add the precursor solution into the syringe of the electrospinning equipment, and spin method, to obtain precursor composite fibers (spinning conditions: spinning voltage 30KV, extrusion speed 2.0ml / min); repeat the above process several times to obtain multiple precursor composite fibers; remove all composite fibers from the receiving plate, and Calcined in a medium-temperature furnace at 1000° C. for 10 hours, collected 38.76 g of zirconium dioxide fiber powder; the average length of the obtained zirconium dioxide fibers was 1.5 microns, and the average diameter was 0.3 microns. Soak the fiber powder in a silane coupling agent solution, filter, and dry to carry out surface lipophilic modification treatment; weigh 25.0 g of the pretreated ...
Embodiment 3
[0032] Example 3: Attapulgite clay fiber separator S3
[0033] The attapulgite clay is selected from the Xuyi area of Jiangsu Province. It is fibrous in shape, with an average length of 1 micron and an average diameter of 0.05 micron. Filtration, drying, and surface lipophilic modification treatment; the main component of attapulgite clay rods is silicon dioxide, weigh 60g of pretreated composite fiber powder, 14g of polyvinylidene fluoride, and 1g of polyethylene glycol, and dissolve them in 75g In ethanol, the slurry is formed after sufficient stirring; the slurry is subjected to vacuum defoaming treatment, and the defoaming slurry is continuously and automatically cast into a film by a tape casting machine and dried to obtain an attapulgite clay with a thickness of 100 microns Fibrous septum.
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