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Initiator-containing abrasive particle-free polishing solution composition for memory hard disk substrate and preparation method thereof

A technology of polishing liquid composition and initiator, which is applied in the direction of polishing composition, chemical instruments and methods, etc., can solve the problems of high hardness, poor dispersion and easy agglomeration of nano-abrasive particles, so as to improve the removal rate and reduce microscopic scratches , Improve the effect of flatness

Inactive Publication Date: 2015-04-08
SHANGHAI UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] The traditional chemical mechanical polishing (CMP) technology is an important means of computer hard disk processing at present. It realizes the removal of materials and the flattening of the surface of the workpiece under the combination of chemical and mechanical effects. Although the material removal rate of the workpiece is high, the polishing process Due to the high hardness of nano-abrasive particles, easy agglomeration, and poor dispersion, the surface of the workpiece is prone to damage such as dents, corrosion, micro-scratches, and particle residues. However, it cannot well meet the current requirements for the surface smoothing process of atomic-level materials on the surface of hard disks.

Method used

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  • Initiator-containing abrasive particle-free polishing solution composition for memory hard disk substrate and preparation method thereof

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Embodiment 1

[0020] In the present embodiment, the composition and weight percent of the non-abrasive polishing liquid composition of the memory hard disk substrate containing initiator are as follows:

[0021] Azobisisopropylamidinoline hydrochloride AIBI 0.01%

[0022] Hydrogen peroxide 5.0%

[0023] Sodium hexametaphosphate 3.0%

[0024] Cetethoxylate Carboxylate 3.0%

[0025] Deionized water 88.99%

[0026] In this embodiment, the preparation method of the abrasive-free polishing liquid composition of the memory hard disk substrate: adopt azobisisopropylamidinoline hydrochloride AIBI as the initiator, use hydrogen peroxide as the oxidizing agent, and use sodium hexametaphosphate As a dispersant, cetyl polyoxyethylene ether carboxylate was used as a surfactant, deionized water was used as a solvent, and the polishing liquid was prepared by fully mixing according to the weight percentage of the polishing liquid components in this embodiment. The specific steps are as follows:

[002...

Embodiment 2

[0030] This embodiment is basically the same as Embodiment 1, especially in that:

[0031] In the present embodiment, the percentage by weight of the azobisisopropylamidinoline hydrochloride AIBI used is 0.02%, the percentage by weight of deionized water is 88.98%, and the remaining components and the memory hard disk substrate containing the initiator The steps of the preparation method of the non-abrasive polishing liquid composition are all the same as those in Embodiment 1.

Embodiment 3

[0033] This embodiment is basically the same as Embodiment 1, especially in that:

[0034] In the present embodiment, the composition and weight percent of the non-abrasive polishing liquid composition of the memory hard disk substrate containing initiator are as follows:

[0035] Azobisisobutyronitrile AIBN 0.01%

[0036] Hydrogen peroxide 5.0%

[0037] Sodium hexametaphosphate 3.0%

[0038] Cetethoxylate Carboxylate 3.0%

[0039] Deionized water 88.99%

[0040] In this embodiment, the preparation method of the non-abrasive polishing liquid composition of the memory hard disk substrate: adopt azobisisobutyronitrile AIBN as the initiator, use hydrogen peroxide as the oxidizing agent, use sodium hexametaphosphate as the dispersant, and use ten Hexaalkyl polyoxyethylene ether carboxylate is used as a surfactant, and deionized water is used as a solvent, and the polishing liquid is fully mixed according to the weight percentage content of the polishing liquid components in t...

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Abstract

The invention discloses an initiator-containing abrasive particle-free polishing solution composition for a memory hard disk substrate. The initiator-containing abrasive particle-free polishing solution composition comprises 0.01-0.12% of an azo initiator, 1.0-6.0% of an oxidizing agent hydrogen peroxide, 1.0-4.0% of a dispersant sodium hexametaphosphate, 1.0-4.0% of a surfactant polyoxypropylene cetyl ether carboxylate and the balance deionized water. The preparation method of the polishing solution composition comprises the following steps of weighing raw materials according to a formula of the polishing solution composition, orderly adding the initiator, the dispersant and the surfactant into the deionized water with stirring, and after stirring dissolution, adding the oxidizing agent into the solution with continuous stirring to obtain a transparent liquid which is the polishing solution composition. The polishing solution composition does not contain particles, contains the initiator, is especially suitable for polishing a Ni-P-coated computer hard disk substrate, can improve a substrate removal rate, can reduce surface microscopic scratches and pits and can improve hard disk substrate surface flatness.

Description

technical field [0001] The invention relates to a polishing liquid and a preparation method thereof, in particular to a non-abrasive polishing liquid for a hard disk substrate and a preparation method thereof, which are applied in the technical field of computer memory hard disk manufacturing and surface polishing. Background technique [0002] In recent years, with the rapid development of information technology, the capacity and storage density of memory hard disks have increased rapidly at a rate of 100-200% per year, and computer hard disks are developing in the direction of larger capacity, smaller volume and lower cost. The magnetic head reads smaller and weaker signals, so the distance between the magnetic head and the magnetic medium of the disk needs to be further reduced to increase the strength of the output signal. At present, the flying height of commercialized computer heads has been reduced to about 3 nanometers. As the magnetic head and the magnetic disk run...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C09G1/18
CPCC09G1/18
Inventor 雷红任小艳陈入领蒋婷王莹马盼王瑶
Owner SHANGHAI UNIV