Metal halide pellet of quartz metal halide lamp and preparation method for metal halide pellet as well as mercury-free quartz metal halide lamp
A technology of metal halide pellets and metal halide lamps, which is applied in the manufacture of discharge tubes/lamps, components of gas discharge lamps, cold cathodes, etc., can solve the problems of tube wall blackening and reduce the luminous flux maintenance rate of lamp tubes, etc. Achieve the effect of good sphericity, excellent photoelectric and color comprehensive parameters, and eliminate the harm of mercury
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Embodiment 1
[0039]A metal halide pellet of a quartz metal halide lamp, the material of which is luminescent metal halide; the material of the luminescent metal halide is a composition of sodium iodide, scandium iodide and calcium iodide; The mass ratio of sodium, scandium iodide and calcium iodide is 4:0.6:1.
[0040] The preparation method of described golden halide pill, comprises the following steps:
[0041] (1) The above-mentioned luminescent metal halides were weighed in proportion, mixed uniformly to form a mixture, and placed in a quartz container with a nozzle; the mixture was pre-vacuumized at 110°C for 40 minutes, and the vacuum degree was 0.01Mpa;
[0042] (2) Under the condition of a vacuum degree of 0.01Mpa, slowly heat the mixture at a heating rate of 1°C / min until it melts, and then continue to stir for 20 minutes, and spray the molten mixture from the nozzle, and the molten beads are in high-purity Rapid cooling and solidification into balls during the argon mass transfe...
Embodiment 2
[0046] A metal halide pill of a quartz metal halide lamp, the material is a complex formed by luminescent metal halide and buffer metal halide; the material of the luminescent metal halide is a combination of sodium iodide, scandium iodide and calcium iodide The material of the buffer metal halide is a mixture of antimony iodide and thulium iodide; the mass ratio of sodium iodide, scandium iodide, calcium iodide, antimony iodide and thulium iodide in the metal halide pellets is 4:0.6:1:2:1.
[0047] The preparation method of described golden halide pill, comprises the following steps:
[0048] (1) The above-mentioned luminescent metal halide and buffer metal halide were weighed in proportion, mixed uniformly to form a mixture, and placed in a quartz container with a nozzle; the mixture was pre-vacuumized at 120°C for 50 minutes, and the vacuum degree was 0.01Mpa;
[0049] (2) Under the condition of a vacuum degree of 0.01Mpa, slowly heat the mixture at a heating rate of 2°C / ...
Embodiment 3
[0053] A metal halide pill of a quartz metal halide lamp, the material is a complex formed by luminescent metal halide and buffer metal halide; the material of the luminescent metal halide is a combination of sodium iodide, scandium iodide and calcium iodide The material of the buffer metal halide is a mixture of antimony iodide and thulium iodide; the mass ratio of sodium iodide, scandium iodide, calcium iodide, antimony iodide and thulium iodide in the metal halide pellets is 8:1.5:1.8:5:2.5.
[0054] The preparation method of described golden halide pill, comprises the following steps:
[0055] (1) The above-mentioned luminescent metal halide and buffer metal halide were weighed in proportion, mixed uniformly to form a mixture, and placed in a quartz container with a nozzle; the mixture was pre-vacuumized at 130°C for 50 minutes, and the vacuum degree was 0.01Mpa;
[0056] (2) Under the condition of a vacuum degree of 0.01Mpa, slowly heat the mixture at a heating rate of ...
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