Preparation method of composite antistatic agent for fiber fabric
A composite antistatic agent and antistatic agent technology, which is applied in fiber treatment, textiles and papermaking, etc., can solve problems such as increased friction coefficient, poor fiber adsorption, and poor antistatic effect, and achieves improved surface conductivity and excellent antistatic properties. Effects of electrostatic properties and good high temperature resistance
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Embodiment 1
[0045] This embodiment provides a method for preparing a composite antistatic agent for fiber fabrics. In the preparation method, the composite antistatic agent for fiber fabrics includes the following components in parts by mass:
[0046]Butanol phosphate antistatic agent: 40 parts, hydroxyl-terminated hyperbranched antistatic agent: 8 parts, carboxyl-terminated hyperbranched antistatic agent: 15 parts, quaternary ammonium salt-terminated hyperbranched antistatic agent: 23 parts;
[0047] The concrete preparation method of this fiber fabric composite antistatic agent is as follows:
[0048] (1) Preparation of Butanol Phosphate Antistatic Agent
[0049] (1) Add n-butanol to a clean three-necked flask, then add phosphorus pentoxide, slowly put it into a three-necked flask with n-butanol with a medicine spoon, and place the three-necked flask in a large beaker filled with cold water to Control its temperature not to exceed 50°C during the addition process;
[0050] The molar r...
Embodiment 2
[0070] This embodiment provides a method for preparing a composite antistatic agent for fiber fabrics. In the preparation method, the composite antistatic agent for fiber fabrics includes the following components in parts by mass:
[0071] Butanol phosphate antistatic agent: 35 parts, hydroxyl-terminated hyperbranched antistatic agent: 5 parts, carboxyl-terminated hyperbranched antistatic agent: 10 parts, quaternary ammonium salt-terminated hyperbranched antistatic agent: 25 parts;
[0072] The concrete preparation method of this fiber fabric composite antistatic agent is as follows:
[0073] (1) Preparation of Butanol Phosphate Antistatic Agent
[0074] (1) Add n-butanol to a clean three-necked flask, then add phosphorus pentoxide, slowly put it into a three-necked flask with n-butanol with a medicine spoon, and place the three-necked flask in a large beaker filled with cold water to Control its temperature not to exceed 50°C during the addition process;
[0075] The molar ...
Embodiment 3
[0095] This embodiment provides a method for preparing a composite antistatic agent for fiber fabrics. In the preparation method, the composite antistatic agent for fiber fabrics includes the following components in parts by mass:
[0096] Butanol phosphate antistatic agent: 38 parts, hydroxyl-terminated hyperbranched antistatic agent: 10 parts, carboxyl-terminated hyperbranched antistatic agent: 13 parts, quaternary ammonium salt-terminated hyperbranched antistatic agent: 20 parts;
[0097] The concrete preparation method of this fiber fabric composite antistatic agent is as follows:
[0098] (1) Preparation of Butanol Phosphate Antistatic Agent
[0099] (1) Add n-butanol to a clean three-necked flask, then add phosphorus pentoxide, slowly put it into a three-necked flask with n-butanol with a medicine spoon, and place the three-necked flask in a large beaker filled with cold water to Control its temperature not to exceed 50°C during the addition process;
[0100] The molar...
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