Method for recovering copper from waste circuit board
A technology for waste circuit boards and ore pulp, applied in the field of hydrometallurgy, can solve the problems of complicated extraction process of metal copper, difficult to achieve large-scale application, increase of processing cost, etc. The effect of reducing recovery costs
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Embodiment 1
[0031] Take 10 grams of a copper-clad circuit board with a copper content of 20.38%, and mechanically crush it to below 200 mesh; at a solid-to-liquid ratio of 1:3, a stirrer speed of 200r / min, a reaction temperature of 25°C, and an air volume of 12m 3 / h, ammonium chloride concentration 1mol / L, ammonia water 1 mol / L, turn on the ultrasonic wave, power 60W, add 1L / t hydrogen peroxide every 20min, ultrasonic enhanced oxidation leaching for 1 hour, the leaching of metal copper in waste copper circuit boards The rate is 98.19%.
Embodiment 2
[0033] Take 10 grams of a copper-clad circuit board with a copper content of 20.98%, and mechanically crush it to below 200 mesh; at a solid-liquid ratio of 1:8, a stirrer speed of 800r / min, and a reaction temperature of 25°C, the amount of air introduced is 12m 3 / h, ammonium chloride concentration 5mol / L, ammonia water 4 mol / L, turn on the ultrasonic wave, power 120W, add 3L / t hydrogen peroxide every 20min, ultrasonic enhanced oxidation leaching for 4 hours; leaching of metal copper in waste copper circuit boards The rate is 99.53%.
Embodiment 3
[0035] Take 10 grams of a copper-clad circuit board with a copper content of 19.58%, and mechanically crush it to below 200 mesh; at a solid-liquid ratio of 1:5, a stirrer speed of 600r / min, a reaction temperature of 25°C, and an air volume of 10m 3 / h, ammonium chloride concentration 3mol / L, ammonia water 2 mol / L, turn on the ultrasonic wave, power 180 W, add 2L / t hydrogen peroxide every 20min, ultrasonic enhanced oxidation leaching for 2 hours; The leaching rate is 98.62%.
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