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Method for preparing titanium product through titanium hydride powder

A technology of powder preparation and titanium hydride, which is applied in the field of preparing titanium products from titanium hydride powder and titanium products. It can solve the problems of high cost of HDH titanium powder, increased cost of parts, and low product density. It achieves low oxygen content, The effect of high density and high mechanical properties

Inactive Publication Date: 2015-11-25
SHANGHAI JIAO TONG UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

However, the dehydrogenation process takes a long time, usually several hours to more than ten hours
In addition, due to the high chemical activity of titanium, it is easy to react with impurity elements such as H, O, C, and N in the environment at high temperatures. Therefore, the requirements for the surrounding environment are strict during the production of titanium powder. High-purity The cost of HDH titanium powder is still high
[0006] Titanium powder will inevitably come into contact with impurity elements in the surrounding environment during subsequent processing and consolidation into parts, thereby reacting with each other and reducing product performance (H, O, C, N and other elements are easy to diffuse into the titanium lattice gap, resulting in reduced shaping of titanium)
In the current research, the titanium products prepared by dehydrogenation using titanium hydride as raw material are easy to form holes in the material due to the precipitation of hydrogen in the form of hydrogen gas, resulting in low density of the final product, and are mostly used to prepare porous materials for medical use
The shape of titanium is strong, the cold working performance is poor, and the subsequent machining is difficult, which further increases the cost of titanium parts

Method used

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  • Method for preparing titanium product through titanium hydride powder
  • Method for preparing titanium product through titanium hydride powder
  • Method for preparing titanium product through titanium hydride powder

Examples

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Effect test

Embodiment 1

[0060] In this example, titanium hydride powder is used as a raw material, and the process and steps of preparing titanium products through rapid dehydrogenation, sintering and extrusion consolidation forming processes under the protection of argon are as follows:

[0061] 1. 50g of titanium hydride powder (-200 mesh) was pressed into a powder compact with a diameter of 28mm and a height of 20mm by one-way molding at room temperature under a pressure of 500MPa.

[0062] 2. In the self-modified induction heating and extrusion equipment, the induction coil and the extrusion device are placed in the same closed glove box. The titanium hydride powder compact is placed in the induction coil. Pass argon gas with a purity of 99.99% into the closed glove box, and use an oxygen analyzer to measure the oxygen content in the glove box until the atmospheric oxygen content in the glove box is lower than 100ppm. During the inflation process, the extrusion cylinder, the extrusion die and th...

Embodiment 2

[0066] 1. 50g of titanium hydride powder (-200 mesh) was pressed into a powder compact with a diameter of 28mm and a height of 19mm by unidirectional molding at 100°C under a pressure of 500MPa.

[0067] 2. In the self-modified induction heating and extrusion equipment, the induction coil and the extrusion device are placed in the same closed glove box. The titanium hydride powder compact is placed in the induction coil. Pass argon gas with a purity of 99.99% into the closed glove box, and use an oxygen analyzer to measure the oxygen content in the glove box until the atmospheric oxygen content in the glove box is lower than 100ppm. During the inflation process, the extrusion cylinder, the extrusion die and the extrusion rod are heated to 500° C. by means of electric heating coils.

[0068] 3. Adjust the power of the medium-frequency induction heating coil to heat the titanium hydride powder compact so that the heating rate is maintained at 100°C / min until the compact tempera...

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Abstract

The invention discloses a method for preparing a titanium product through titanium hydride powder. The method comprises the following steps that firstly, blank manufacturing is carried out, and the titanium hydride powder is manufactured into a blank material through mold pressing; secondly, dehydrogenation is carried out, the blank material is heated under the protective atmosphere, the temperature rise rate is maintained in 50-200 DEG C / min till the temperature of the blank material is increased to 900-1,200 DEG C, and insulating is carried out for 5-20 minutes; thirdly, molding is carried out, the heated blank material is moved in an extrusion device, extrusion is carried out under a certain pressure and extrusion ratio, and the blank material is molded and solidified to obtain the titanium product through an extrusion mold with a specific inner cavity shape; and fourthly, cooling is carried out, and after extrusion is finished, the titanium product is cooled to the room temperature at the speed of 10-100 DEG C / min and then taken out. The method has the beneficial effects that the cost of raw materials is low, the dehydrogenation speed is high, and the production efficiency and product purity are high; and the technological process is simple, and the large-scale production potential is achieved.

Description

technical field [0001] The invention relates to a method for preparing titanium products, in particular to a method for preparing titanium products by using titanium hydride powder, and belongs to the technical field of nonferrous metal processing. Background technique [0002] As an important non-ferrous metal material, titanium and titanium alloys have been widely used in aerospace vehicles, ships and It is widely used in the manufacture of weapons and other military products. In addition, titanium also has great application potential in industries such as automobile, medical treatment, chemical industry, energy and daily consumption. Therefore, titanium is also called "the rising third metal" and "the metal of the 21st century". [0003] However, due to the high chemical activity of titanium, the difficulty of smelting, high energy consumption, and its poor cold working performance, the production cost of titanium is high, which limits its further application range. In ...

Claims

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Application Information

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IPC IPC(8): B22F3/00B22F3/20
Inventor 张德良郑逸锋梁加淼周登山
Owner SHANGHAI JIAO TONG UNIV
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