A kind of preparation method of antiglare glass with high toughness and high hardness
A technology of anti-glare glass and high hardness, which is applied in the field of glass preparation and can solve problems such as unsatisfactory toughness and hardness
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[0021] refer to figure 1 , the present invention proposes a method for preparing anti-glare glass with high toughness and high hardness, comprising the following steps:
[0022] S1. Weigh 1.5-2.6% aluminum oxide, 15-28% iron oxide, 1.2-3.8% magnesium oxide, 2.2-3.8% zinc oxide, 1.5-12.5% calcium oxide, 1.2-2.4% calcium fluoride, 1.3-2.7% yttrium trioxide, 1.8-2.2% zirconia, 2.4-4.8% antimony trioxide, 2.2-4.8% boron trioxide, 1.5-3.5% phosphorus pentoxide, 10.2-18.8% sodium oxide , the balance is silica powder, after mixing evenly, grind to obtain the mixture;
[0023] S2. Put the mixture obtained in S1 in a melting furnace and heat it up to 1650-1700°C, keep it warm for 2-4 hours, add a compound clarifying agent for clarification, and then air-cool to room temperature to obtain material a, wherein the concentration of the compound clarifying agent is 32-42wt% Sodium antimonate solution;
[0024] S3. Form material a, then perform annealing treatment, and air cool to room ...
Embodiment 1
[0028] The present invention proposes a method for preparing anti-glare glass with high toughness and high hardness, comprising the following steps:
[0029] S1. Weigh 2.05% aluminum oxide, 21.5% iron oxide, 2.5% magnesium oxide, 3.0% zinc oxide, 7.0% calcium oxide, 1.8% calcium fluoride, 2.0% yttrium trioxide, 2.0% zirconium dioxide by weight percentage , 3.6% antimony trioxide, 3.5% diboron trioxide, 2.5% phosphorus pentoxide, 14.5% sodium oxide, and the balance is silicon micropowder. After mixing evenly, grind to obtain a mixture;
[0030] S2. Put the mixture obtained in S1 in a melting furnace to heat up to 1675° C., keep it warm for 3 hours, add a sodium antimonate solution with a concentration of 37 wt % for clarification, and air-cool to room temperature to obtain material a;
[0031] S3. Form material a, then heat up to 195°C, keep warm for 55min, air cool to room temperature, then heat up to 260°C, keep warm for 55min, air cool to room temperature, then heat up to 30...
Embodiment 2
[0035] The present invention proposes a method for preparing anti-glare glass with high toughness and high hardness, comprising the following steps:
[0036] S1. Weigh 1.5% alumina, 28% iron oxide, 1.2% magnesium oxide, 3.8% zinc oxide, 1.5% calcium oxide, 2.4% calcium fluoride, 1.3% yttrium trioxide, 2.2% zirconium dioxide by weight percentage , 2.4% antimony trioxide, 4.8% diboron trioxide, 1.5% phosphorus pentoxide, 18.8% sodium oxide, and the balance is silicon micropowder. After mixing evenly, grind to obtain a mixture;
[0037]S2. Put the mixture obtained in S1 in a melting furnace and heat it up to 1700° C., keep it warm for 2 hours, add a sodium antimonate solution with a concentration of 42 wt% for clarification, and then air-cool to room temperature to obtain material a;
[0038] S3. Mold material a, then heat up to 210°C, keep warm for 40 minutes, air cool to room temperature, then heat up to 210°C, keep warm for 70 minutes, air cool to room temperature, then heat u...
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