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Preparation method of high temperature resistant medical deodorization material

A deodorant material and high temperature resistant technology, applied in the field of medical materials, can solve the problems of poor light and thermal stability, inability to achieve good application stability, discoloration, etc., and achieve the effect of good performance and significant deodorization performance.

Inactive Publication Date: 2015-12-09
JIANGSU LANWAN BIOTECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, it has poor stability to light and heat. When it is above 100°C or exposed to the sun for a long time, it will decompose to produce hydrogen chloride, and further autocatalyze the decomposition, causing discoloration and rapid decline in physical and mechanical properties. In practical applications, stabilizer must be added. agent to improve heat and light stability
In the medical field, due to the particularity of the use environment, there are more application requirements for PVC materials, such as high temperature resistance, deodorization, etc., but currently commonly used PVC materials cannot achieve high temperatures in high temperature environments. Good application stability, and deodorization performance is rarely involved, which requires the development of a composite material with a variety of special properties to meet the needs of the medical field

Method used

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  • Preparation method of high temperature resistant medical deodorization material

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0019] A preparation method of a high temperature resistant medical deodorant material, comprising the following preparation steps:

[0020] Step 1: Add 10 parts by weight of PVC, 2 parts of PET, 1 part of dioctyl phthalate, 0.8 part of lecithin, 3 parts of polycarbonate and 1 part of barium stearate into a mixing mixer and stir to mix evenly , the stirring speed was 160 rev / min, the stirring time was 20 minutes, and the material 1 was obtained;

[0021] Step 2: Add material 1 to the reaction kettle, add 1 part of glass fiber in parts by weight, 0.8 part of methyltetrahydrophthalic anhydride, 1 part of aluminum oxide, 2 parts of polyester fiber, 3-propane- 0.5 parts of potassium 2-alkenoyloxypropane-1-sulfonate, heated to 60°C under negative pressure of 0.01MPa, stirred for 2 hours, then heated to 90°C under normal pressure, stirred for 30 minutes , down to 0°C at a cooling rate of 20°C / min, and kept at 0°C for 10 minutes to obtain material 2;

[0022] Step 3, drying the mat...

Embodiment 2

[0026] A preparation method of a high temperature resistant medical deodorant material, comprising the following preparation steps:

[0027] Step 1: Add 13 parts of PVC in parts by weight, 3 parts of PET, 2 parts of dioctyl phthalate, 1 part of lecithin, 4 parts of polycarbonate and 2 parts of barium stearate into a mixing mixer and stir to mix evenly , the stirring speed was 165 rev / min, the stirring time was 23 minutes, and the material 1 was obtained;

[0028] Step 2: Add material 1 to the reactor, add 2 parts by weight of glass fiber, 1 part of methyltetrahydrophthalic anhydride, 2 parts of aluminum oxide, 3 parts of polyester fiber, 3-propane- 0.6 parts of potassium 2-alkenoyloxypropane-1-sulfonate, heated to 63°C under a negative pressure of 0.02MPa, stirred for 3 hours, then heated to 94°C under normal pressure, stirred for 36 minutes , down to 0°C at a cooling rate of 22°C / min, and kept at 0°C for 13 minutes to obtain material 2;

[0029] Step 3, drying material 2 at...

Embodiment 3

[0033] A preparation method of a high temperature resistant medical deodorant material, comprising the following preparation steps:

[0034] Step 1: Add 18 parts by weight of PVC, 5 parts of PET, 3 parts of dioctyl phthalate, 1.3 parts of lecithin, 7 parts of polycarbonate and 2 parts of barium stearate into a mixing mixer and stir to mix evenly , the stirring speed was 170 rpm, and the stirring time was 28 minutes to obtain material 1;

[0035] Step 2: Add material 1 to the reactor, add 2 parts by weight of glass fiber, 1.2 parts of methyltetrahydrophthalic anhydride, 3 parts of aluminum oxide, 4 parts of polyester fiber, 3-propane- 0.7 parts of potassium 2-alkenoyloxypropane-1-sulfonate, heated to 68°C under a negative pressure of 0.03MPa, stirred for 3 hours, then heated to 96°C under normal pressure, stirred for 45 minutes , down to 0°C at a cooling rate of 23°C / min, and kept at 0°C for 16 minutes to obtain material 2;

[0036] Step 3, drying the material 2 at a drying t...

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Abstract

The invention discloses a preparation method of a high temperature resistant medical deodorization material. The preparation method comprises the steps of firstly adding PVC, PET, dioctyl phthalate, lecithin, polycarbonate and barium stearate into a mixer, stirring and mixing uniformly, then adding the mixture into a reaction still, adding fiberglass, 3a-methyl-5,6-dihydro-4H-isobenzofuran-1,3-dione, aluminium oxide, polyester fiber and potassium 3-sulphonatopropyl acrylate, heating and stirring under a negative pressure condition, then performing temperature rise reaction under a normal pressure condition, then cooling to 0 DEG C, then drying, smashing, stifling by using ammonia gas, and then performing extrusion molding in a twin-screw extruder, thus obtaining the high temperature resistant medical deodorization material. The high temperature resistant medical deodorization material prepared by the preparation method provided by the invention has good high temperature resistance and deodorization performance, thus further expanding the application of the material.

Description

technical field [0001] The invention belongs to the field of medical materials, in particular to a preparation method of a high-temperature-resistant medical deodorant material. Background technique [0002] Polyvinyl chloride, referred to as PVC in English, is a thermoplastic resin polymerized by vinyl chloride under the action of an initiator. It is a homopolymer of vinyl chloride. Vinyl chloride homopolymers and vinyl chloride copolymers are collectively referred to as vinyl chloride resins. PVC is a white powder with an amorphous structure and a small degree of branching. The molecular weight of industrially produced PVC is generally in the range of 50,000 to 120,000, with a large polydispersity, and the molecular weight increases with the decrease of the polymerization temperature; there is no fixed melting point, it starts to soften at 80-85°C, and becomes viscoelastic at 130°C , 160 ~ 180 ℃ began to change into a viscous flow state; good mechanical properties, tens...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C08L27/06C08L67/02C08L69/00C08K13/04C08K5/12C08K5/098C08K7/14C08K5/09C08K5/42B29C47/92B29C48/92
Inventor 章祥庆唐海健
Owner JIANGSU LANWAN BIOTECH
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