Preparation method of calcium amino acid chelate
A technology for chelating calcium and amino acids, which is applied in the preparation of organic compounds, chemical instruments and methods, and cyanide reaction preparation, etc., can solve the problems of incapable of large-scale production, low complexation rate, and low dissolved concentration, and achieve increased Yield, simplification of operation process, significant absorption effect
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example 1
[0019] First, take 600g of egg shells and put them into a pulverizer to crush them, and sieve them to obtain 80 mesh powders, put the obtained powders into a container, add a hydrochloric acid solution with a mass fraction of 60% to soak the powders, and stir for 20 minutes at 400r / min Finally, filter to obtain the filtrate; then put the above-mentioned filtrate into a container, add 60mL of egg white and 40g of proteolytic enzyme to it respectively, use a sodium hydroxide solution with a mass fraction of 30% to adjust the pH to 6.5, and then use Heat it with microwave, after heating to 35°C, add 40g of zinc acetate to it, and stir for 20min; then, after the above stirring is completed, electrify the solution so that the current of the solution in the container is 25mA, let it stand for 15min, and put the container The mixture in the centrifuge is poured into the centrifuge for centrifugation, and the centrifuge is collected for later use; then the above-mentioned centrifuged l...
example 2
[0022] First, take 700g of egg shells and put them into a pulverizer to crush them, and sieve them to obtain 90-mesh powder. Put the obtained powder into a container, add a hydrochloric acid solution with a mass fraction of 60% to soak the powder, and stir for 25 minutes at 450r / min. Finally, filter to obtain the filtrate; then put the above-mentioned filtrate into a container, add 80mL of egg white and 50g of proteolytic enzyme to it respectively, use a sodium hydroxide solution with a mass fraction of 30% to adjust the pH to 6.8, and then use Heat it with microwave, after heating to 40°C, add 45g of zinc acetate to it, and stir for 30min; then, after the above stirring is completed, electrify the solution so that the current of the solution in the container is 35mA, let it stand for 18min, and put the container The mixture in the centrifuge is poured into the centrifuge for centrifugation, and the centrifuge is collected for later use; then the above-mentioned centrifuged liq...
example 3
[0025]First, take 800g of egg shells and put them into a pulverizer for crushing, and sieve to obtain a 100-mesh powder. Put the obtained powder into a container, add a hydrochloric acid solution with a mass fraction of 60% to soak the powder, and stir for 30 minutes at 500r / min. Finally, filter to obtain the filtrate; then put the above-mentioned filtrate into a container, add 90mL egg white and 60g proteolytic enzyme therein respectively, use a 30% sodium hydroxide solution to adjust the pH to 7.0, and then use Heat it with microwave, after heating to 45°C, add 50g of zinc acetate to it, and stir for 40min; then, after the above stirring is completed, electrify the solution so that the current of the solution in the container is 40mA, let it stand for 20min, and put the container The mixture in the centrifuge is poured into the centrifuge for centrifugation, and the centrifuge is collected for later use; then the above-mentioned centrifuged liquid is put into a container, and...
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