Rapidly cured rigid polyurea with high adhesion and preparation method of rapidly cured rigid polyurea
A high-adhesion, fast-curing technology, used in polyurea/polyurethane coatings, coatings, etc., can solve problems such as difficulty in adapting to working conditions, uneven adhesion, and few applications, shortening gel time, The effect of increasing the crosslinking density and broadening the application field
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specific Embodiment 1
[0031] A fast-curing high-adhesion rigid polyurea is a two-component component, and the mass percentages of the raw materials of component A and component B are as follows:
[0032] Preparation of component A: Add 30 parts of polytetrahydrofuran polyol PTMEG1000 into the reaction kettle, 110~120°C, vacuum -0.08~-0.1MPa, stir and dehydrate for 2~3 hours, remove the vacuum and cool down to below 60°C, add 63 parts of For MDI-100, heat to 80-90°C and keep it warm for 2-3 hours, then add 7 parts of coupling agent KH560 after cooling, stir and discharge evenly.
[0033] Preparation of component B: 30 parts of DETDA, 45 parts of polytetrahydrofuran polyol PTMEG1000, 15 parts of dehydrated castor oil, 0.3 parts of dibutyltin dilaurate, 1 part of antioxidant 1010, 1 part of UV-531, 1 part of wetting Add dispersant BYK104S, 1.2 parts of leveling agent BYK203, 1 part of titanium dioxide, and 4.5 parts of dewatering agent 3A activation powder into the tank, disperse at high speed for 0.5...
specific Embodiment 2
[0037] A fast-curing high-adhesion rigid polyurea is a two-component component, and the mass percentages of the raw materials of component A and component B are as follows:
[0038] Preparation of component A: Add 40 parts of polyoxypropylene glycol PPG2000 into the reaction kettle, 110~120°C, vacuum -0.08~-0.1MPa, stir and dehydrate for 2~3 hours, remove the vacuum and cool down to below 60°C, add 35 1 part of MDI-50, 25 parts of polyphenylmethane polyisocyanate PAPI, heated to 80-90 ℃ and kept for 2-3 hours, then cooling and adding 5 parts of coupling agent KH560, stirring evenly and discharging. Preparation of component B: 30 parts of DETDA, 35 parts of polytetrahydrofuran polyol PTMEG1000, 25 parts of polyethylene glycol, 0.3 part of dibutyltin dilaurate, 1 part of antioxidant 1010, 1 part of UV-531, 1 part of moisturizing Wet dispersant BYK104S, 1.2 parts of leveling agent BYK203, 1 part of titanium dioxide, 4.5 parts of dewatering agent 3A activation powder were added to...
specific Embodiment 3
[0043] A fast-curing high-adhesion rigid polyurea is a two-component component, and the mass percentages of the raw materials of component A and component B are as follows:
[0044] Preparation of component A: 40 parts of polyoxypropylene glycol PPG1000, 110~120°C, vacuum -0.08~-0.1MPa, stirring and dehydrating for 2~3 hours, after removing the vacuum, cool down to below 60°C and add 45 parts of MDI- 50,15 parts of MDI-100LL are heated to 80-90°C and kept for 2-3 hours, then cooled and added with 5 parts of coupling agent KH560, stirred evenly and discharged. Preparation of component B: 20 parts of DETDA, 35 parts of polytetrahydrofuran polyol, 25 parts of 4,4-bis-sec-butylaminodiphenylmethane, 0.3 parts of dibutyltin dilaurate, 1 part of antioxidant 1010, 1 part Add UV-531, 1 part of wetting and dispersing agent BYK2008, 1.2 parts of leveling agent BYK110, 1 part of titanium dioxide, and 4.5 parts of dewatering agent 3A activation powder into the pulling tank, disperse at h...
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