Feeding microelement amino acid chelate additive and preparation method thereof

A technology of trace elements and amino acids, applied in application, animal feed, additional food elements, etc., can solve the problems of poor use effect, reduction and loss of chelation strength and chelation rate, and achieve improved bioavailability and dispersion performance, easy operation

Inactive Publication Date: 2016-06-01
河南艾德昕生物科技有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0002] Trace element amino acid chelate is a new type of feed additive developed in recent years to replace inorganic trace elements. It is because amino acid ligands (glycine, lysine, methionine, etc.) 2+ 、Cu 2+ , Zn 2+ , Mn 2+ ) chelation, so that trace elements can improve the bioavailability of trace elements by means of amino acid absorption channels, however, the chelation strength of amino acids and trace elements is not high, and the pKd is about 6-8 under neutral conditions, especially in acidic conditions Down, H + It will compete with metal ions for the electron-donating groups of amino acids, resulting in a significant reduction in the chelation strength and chelation rate of trace element amino acid chelates
[0003] The pH value of animal gastric juice is around 1-2, the chelation rate of amino acid chelate of trace elements in the stomach will drop to 20-40%, and more than 60% of trace element ions will dissociate from amino acid ligands and be in free form. After entering the small intestine, as the pH of the digestive tract increases, the free trace element ions will combine with phosphate, phytic acid, polyphenols, etc. with higher affinity to form insoluble complexes, resulting in the inability of most trace elements to be absorbed and utilized
Amino acid chelation loses its meaning because it cannot be combined with amino acid again, which is also an important reason why many trace element amino acid chelates are not effective in actual use.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0026] The feed trace element amino acid chelate additive in this embodiment is prepared by wrapping the glyceryl monostearate layer and the glyceryl monolaurate layer successively from the inside to the outside on the surface of ferrous glycinate; wherein the parts by weight of each raw material Dosage: 5 parts of ferrous glycinate, 1 part of glyceryl monostearate, and 1 part of glyceryl monolaurate.

[0027] The preparation method of the feed trace element amino acid chelate additive in this embodiment, the specific operation steps are:

[0028] 1) Pass ferrous glycinate through a 100-mesh sieve, mix evenly with glyceryl monostearate, place in a microwave machine, heat to 80°C at 915MHz, heating power 20Kw, and stir at 20r / min for 20min to obtain mixture 1;

[0029] 2) Cool the mixture 1 to 50°C, keep stirring at 90r / min, add glyceryl monolaurate, mix evenly, heat to 63°C with microwave at 915MHz, 20Kw, stir and react at 20r / min for 20min, to obtain mixture 2;

[0030] 3) ...

Embodiment 2

[0033] This embodiment feeds the trace element amino acid chelate additive, which is prepared by wrapping the glyceryl monostearate layer and the glyceryl monolaurate layer on the surface of copper methionine from inside to outside in turn; wherein the parts by weight of each raw material are used It is: 6 parts of copper methionine, 1.5 parts of glyceryl monostearate, and 1.5 parts of glyceryl monolaurate.

[0034] The preparation method of the feed trace element amino acid chelate additive in this embodiment, the specific operation steps are:

[0035] 1) Pass copper methionine through a 200-mesh sieve, mix evenly with glyceryl monostearate, place in a microwave machine, heat to 78°C at 915MHz, heating power 15Kw, and stir at 25r / min for 17min to obtain a mixture 1;

[0036] 2) Cool the mixture 1 to 55°C, keep stirring at 100r / min, add glyceryl monolaurate, mix evenly, microwave heating to 70°C at 915MHz, 15Kw, and stir at 25r / min for 17min to obtain mixture 2;

[0037] 3) ...

Embodiment 3

[0040] The feed trace element amino acid chelate additive in this embodiment is prepared by wrapping glyceryl monostearate layer and glyceryl monolaurate layer successively from inside to outside on the surface of manganese methionine manganese and manganese glycinate mixture; wherein each raw material The dosage in parts by weight is: 4 parts of manganese methionine, 3 parts of manganese glycinate, 2 parts of glyceryl monostearate and 2 parts of glyceryl monolaurate.

[0041] The preparation method of the feed trace element amino acid chelate additive in this embodiment, the specific operation steps are:

[0042] 1) Pass copper methionine and manganese glycinate through a 150-mesh sieve, mix evenly with glyceryl monostearate, place in a microwave machine, heat to 88°C at 915MHz, heating power 30Kw, and stir at 30r / min for 15min , to get mixture 1;

[0043] 2) Cool the mixture 1 to 52°C, keep stirring at 120r / min, add glyceryl monolaurate, mix evenly, microwave heating to 73°...

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PUM

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Abstract

The invention relates to the technical field of feed additive pretreatment, and particularly discloses a feeding microelement amino acid chelate additive and a preparation method thereof. The additive is prepared by coating the surface of a microelement amino acid chelate with a glycerin monostearate layer and a monolaurin layer in sequence from inside to outside, wherein the parts by weight of all raw materials are 5-7 parts of the microelement amino acid chelate, 1-2 parts of glycerin monostearate and 1-2 parts of monolaurin. Both the glycerin monostearate and the monolaurin have strong acid resistance, and separate the dissociation of gastric acid to the microelement amino acid chelate; after the additive enters the intestinal tract, the coating layers are digested, further the microelement amino acid chelate inside is released and is quickly absorbed and utilized, and the bioavailability of the microelement amino acid chelate is increased. The preparation method is simple and convenient to operate, easy to control, and suitable for industrial popularization and application.

Description

technical field [0001] The invention relates to the technical field of feed additive pretreatment, in particular to a trace element amino acid chelate additive for feed and a preparation method thereof. Background technique [0002] Trace element amino acid chelate is a new type of feed additive developed in recent years to replace inorganic trace elements. It is because amino acid ligands (glycine, lysine, methionine, etc.) 2+ 、Cu 2+ , Zn 2+ , Mn 2+ ) chelation, so that trace elements can improve the bioavailability of trace elements by means of amino acid absorption channels, however, the chelation strength of amino acids and trace elements is not high, and the pKd is about 6-8 under neutral conditions, especially in acidic conditions Down, H + It will compete with metal ions for the electron-donating groups of amino acids, resulting in a significant reduction in the chelation strength and chelation rate of the trace element amino acid chelate. [0003] The pH value o...

Claims

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Application Information

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IPC IPC(8): A23K20/158A23K20/10
Inventor 刘俊奇周鑫磊李振田
Owner 河南艾德昕生物科技有限公司
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