Overall hydrophobic timber and preparation method thereof
A wood and hydrophobic technology, applied in wood treatment, wood impregnation, wood impregnation, etc., can solve the problems of high price, difficult industrialization, complicated preparation process, etc., and achieve easy realization of reaction conditions, short preparation period, and good controllability. Effect
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Embodiment 1
[0029] A preparation method for integral hydrophobic wood, comprising the steps of:
[0030] (1) Place the sawn fast-growing poplar (specification R×T×L: 20mm×20mm×10mm) in a Soxhlet extractor, and extract it with a mixture of toluene, acetone and ethanol at a volume ratio of 4:1:1 Extract the wood for 8 hours, take out the wood and place it in an electric blast drying oven, dry it at 105±2°C, and set it aside;
[0031] (2) Dissolve 40g of octadecyl isocyanate in 360g of anhydrous dimethylformamide, then place the dried wood in the mixed solution of the two, vacuum impregnate for 30min, and then introduce the wood together with the mixed solution into the reactor , at 100°C for 8 hours;
[0032] (3) Take out the wood from the reaction kettle, place it in a Soxhlet extractor, extract it with a mixed extract of toluene, acetone, and ethanol at a volume ratio of 4:1:1, and extract the wood for 8 hours. Take out the wood and dry it at 105±2°C Instantly.
Embodiment 2
[0034] A kind of preparation method of overall hydrophobic wood, with embodiment 1, its difference is only: (1) the specification of wood is R * T * L: 20mm * 20mm * 20mm; (2) in the mixed solution of step (2) add There are 4g (1%) dibutyltin dilaurate.
Embodiment 3
[0036] A kind of preparation method of overall hydrophobic wood, with embodiment 1, its difference is only: the consumption of anhydrous dimethylformamide is 400g.
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