Preparation method for CuO nanoflake powdery material
A technology of powder materials and nanosheets, applied in the direction of electrolysis process, electrolysis components, etc., can solve the problems of complex preparation process, complicated preparation steps, low output, etc., and achieve the effects of simplified preparation process, environmental friendliness and high output
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Image
Examples
Embodiment 1
[0021] CuO nanosheets (electrolyte is 1mol L -1 NaOH) preparation
[0022] (1) Two basically identical copper sheets are used as two electrodes, with 1mol L -1 NaOH solution is the electrolyte solution, under the action of AC voltage of about 10V and frequency of 50Hz, react at 20°C for 8h, and let it stand for a while after the reaction;
[0023] (2) The product obtained in the above step (1) was centrifuged (8000 rpm), washed with deionized water and ethanol step by step, and vacuum-dried (dried at 100° C. for 12 h) to obtain CuO nanosheet powder material. The X-ray diffraction pattern of CuO nanosheet powder material is as follows: figure 1 As shown, it can be seen from the figure that it has a single CuO diffraction peak, indicating that the powder material is a high-purity CuO crystal phase. The morphology of CuO nanosheet powder material is as follows: figure 2 shown, from figure 2 It can be seen that the CuO material presents a regular sheet-like structure.
Embodiment 2
[0025] CuO nanosheets (electrolyte is 1mol L -1 Preparation of KOH)
[0026] (1) Two basically identical copper sheets are used as two electrodes, with 1mol L -1 KOH solution is the electrolyte solution, under the action of AC voltage of about 15V and frequency of 50Hz, react at 30°C for 8h, and let it stand for a while after the reaction;
[0027] (2) The product obtained in the above step (1) was centrifuged (8000 rpm), washed with deionized water and ethanol step by step, and vacuum-dried (dried at 100° C. for 12 h) to obtain CuO nanosheet powder material. The morphology of CuO nanosheet powder material is as follows: image 3 shown, from image 3 It can be seen that the CuO material presents a regular sheet-like structure.
Embodiment 3
[0029] CuO nanosheets (electrolyte is 1mol L -1 NaOH and KOH mixed system) preparation
[0030] (1) Two basically identical copper sheets are used as two electrodes, with 1mol L -1 In the mixed electrolyte system of NaOH and KOH, under the action of AC voltage of about 15V and frequency of 50Hz, react at 40°C for 8h, and stand for a while after the reaction;
[0031] (2) The product obtained in the above step (1) was centrifuged (8000 rpm), washed with deionized water and ethanol step by step, and vacuum-dried (dried at 100° C. for 12 h) to obtain CuO nanosheet powder material.
[0032] The transmission electron microscope image of CuO nanosheet powder material is as follows Figure 4 shown, from Figure 4 The sheet-like structure of the CuO material can be seen in .
PUM
Login to View More Abstract
Description
Claims
Application Information
Login to View More