Textile printing and dyeing auxiliary agent and preparation method thereof
A technology for textile printing and dyeing and auxiliaries, which is applied in the field of textile printing and dyeing auxiliaries and its preparation, and can solve problems such as increased industrial waste water, waste gas emissions, aggravated pollution, and poor performance
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[0009] The preparation method of described textile printing and dyeing auxiliary agent comprises the following steps:
[0010] ( 1 ) Weigh each raw material according to parts by weight;
[0011] ( 2 ) Mix cocamidopropyl dimethylamine, polyvinylpyridine, ammonium dodecylbenzenesulfonate, polyethylene glycol diacrylate, laurate, styrene maleic anhydride resin, add 10% of NaOH Solution adjustment pH to 8.5 ,exist 7500-8500 r / m Stir in the state 6-10h ;
[0012] ( 3 ) to heat the stirred mixture to 65-75 ℃, then add sodium sulfite, sodium oleoylamino acid, zinc sulfate, barium chloride, conduct the first ultrasonic in an ultrasonic machine, then add cross-linking agent, softener, conduct the second ultrasonic to obtain the finished product.
[0013] Preferably, the steps ( 3 ) in the first ultrasonic power is 800w , the ultrasonic time is 6-7h , the second ultrasonic power is 950w , the ultrasonic time is 4-5h 。
[0014] Com...
Embodiment 1
[0019] ( 1 ) by weighing cocamidopropyl dimethylamine according to parts by weight 50 parts, polyvinylpyridine 45 parts, ammonium dodecylbenzenesulfonate 30 parts, sodium sulfite 30 Parts, Sodium Oleoyl Amino Acid 25 parts, polyethylene glycol diacrylate 20 parts, laurate 20 parts, styrene maleic anhydride resin 15 parts, zinc sulfate 5 parts, barium chloride 5 parts, polyisocyanate 5 parts, silicone oil softener 5 share;
[0020] ( 2 ) Mix cocamidopropyl dimethylamine, polyvinylpyridine, ammonium dodecylbenzenesulfonate, polyethylene glycol diacrylate, laurate, styrene maleic anhydride resin, add 10% of NaOH Solution adjustment pH to 8.5 ,exist 7500 r / m Stir in the state 6h ;
[0021] ( 3 ) to heat the stirred mixture to 65 ℃, then add sodium sulfite, sodium oleoyl amino acid, zinc sulfate, barium chloride, and conduct the first ultrasonic in the ultrasonic machine, the ultrasonic power is 800w , the ultr...
Embodiment 2
[0024] ( 1 ) by weighing cocamidopropyl dimethylamine according to parts by weight 55 parts, polyvinylpyridine 50 parts, ammonium dodecylbenzenesulfonate 35 parts, sodium sulfite 35 Parts, Sodium Oleoyl Amino Acid 30 parts, polyethylene glycol diacrylate 25 parts, laurate 25 parts, styrene maleic anhydride resin 20 parts, zinc sulfate 10 parts, barium chloride 10 Parts, polyether amino modified polysiloxane 7 Parts, Esterquat 7 share;
[0025] ( 2 ) Mix cocamidopropyl dimethylamine, polyvinylpyridine, ammonium dodecylbenzenesulfonate, polyethylene glycol diacrylate, laurate, styrene maleic anhydride resin, add 10% of NaOH Solution adjustment pH to 8.5 ,exist 8000 r / m Stir in the state 8h ;
[0026] ( 3 ) to heat the stirred mixture to 70 ℃, then add sodium sulfite, sodium oleoyl amino acid, zinc sulfate, barium chloride, and conduct the first ultrasonic in the ultrasonic machine, the ultrasonic power is 800w...
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