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Embedded nano iron/two microbial agents and preparation method thereof

A microbial agent and nano-iron technology, which is applied in the field of triclosan wastewater treatment, can solve the problems of poor stability of nano-zero-valent iron, achieve the effects of low microbial toxicity, in-situ repair, and wide sources

Active Publication Date: 2016-09-07
SOUTH CHINA UNIV OF TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Although nano-zero valent iron has many advantages, it still encounters some problems in the process of its application, such as the poor stability of nano-zero valent iron.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0036] (1) Preparation of triclosan-degrading bacterial liquid

[0037] Pick two rings of Pseudomonas putida. and Pseudomonas stutzeri. respectively, and transfer them to 30 mL of nutrient solution, and culture the bacteria at 35°C for 2 days to 10% by volume was inoculated into the proliferation medium, cultured at 35° C. for 2 days, centrifuged at 5000 rpm for 15 minutes, and the logarithmic growth phase cells of the above bacteria were obtained respectively.

[0038] The logarithmic growth phase cells of the above-mentioned thalli are taken out, and with phosphate buffer (its main component sodium chloride 9.0g / L, potassium chloride 0.3g / L, dipotassium hydrogen phosphate 1.2g / L and potassium dihydrogen phosphate 0.3g / L, the rest is water) and washed twice. According to volume percentage, 37% of Pseudomonas putida and 63% of Pseudomonas stutzeri were mixed to obtain Pseudomonas stutzeri thallus for triclosan degradation. The bacteria were suspended in saline and refrigerat...

Embodiment 2

[0053] (1) Preparation of triclosan-degrading bacterial liquid

[0054] Pick two rings of Pseudomonas putida. and Pseudomonas stutzeri. respectively, and transfer them to 30 mL of nutrient solution, and culture the bacteria at 35°C for 2 days to 10% by volume was inoculated into the container of the proliferation medium, cultured at 35° C. for 2 days, centrifuged at 5000 rpm for 15 minutes, and the logarithmic growth phase cells of the above bacteria were obtained respectively.

[0055] The logarithmic growth phase cells of the above-mentioned thalli are taken out, and with phosphate buffer (its main component sodium chloride 9.0g / L, potassium chloride 0.3g / L, dipotassium hydrogen phosphate 1.2g / L and potassium dihydrogen phosphate 0.3g / L, the rest is water) and washed twice. According to volume percentage, 37% of Pseudomonas putida and 63% of Pseudomonas stutzeri were mixed to obtain Pseudomonas stutzeri thallus for triclosan degradation. The bacteria were suspended in sali...

Embodiment 3

[0069] (1) Preparation of triclosan-degrading bacterial liquid

[0070] Pick two rings of Pseudomonas putida. and Pseudomonas stutzeri. respectively, and transfer them to 30 mL of nutrient solution, and culture the bacteria at 35°C for 2 days to 10% was inoculated into the container of the proliferation medium, cultured at 35° C. for 2 days, centrifuged at 5000 rpm for 15 minutes, and the logarithmic growth phase cells of the above bacteria were obtained respectively.

[0071] The logarithmic growth phase cells of the above-mentioned thalli are taken out, and with phosphate buffer (its main component sodium chloride 9.0g / L, potassium chloride 0.3g / L, dipotassium hydrogen phosphate 1.2g / L and potassium dihydrogen phosphate 0.3g / L, the rest is water) and washed twice. According to volume percentage, 37% of Pseudomonas putida and 63% of Pseudomonas stutzeri were mixed to obtain Pseudomonas stutzeri thallus for triclosan degradation. The bacteria were suspended in saline and ref...

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Abstract

The invention discloses an embedded nano iron / two microbial agents and a preparation method thereof. The preparation method comprises the following steps of: firstly preparing thalli A of two microbial agents by utilizing Pseudomonas putida and Pseudomonas Stutzeri. 2 rings; preparing nano iron solution B, preparing an embedding agent agar, PVA and SiO2 solution C, and preparing a crosslinking agent aluminum sulphate saturated boric acid solution D; and respectively taking 15-18% of the solution B and 6-15% of the thalli A in volume ratio, adding into 57-66% of the solution C, stirring and uniformly mixing, dropwise adding into 1-22% of the solution D at room temperature in a nitrogen protection environment, then carrying out crosslinking treatment, cleaning, and storing, so that the nano iron / two microbial agents are obtained. The preparation method disclosed by the invention utilizes synergistic effect of the nano iron and microorganisms, degradation efficiency of triclosan is improved, and the obtained microbial agent is high in strength, low in microorganism toxicity, available in raw materials and low in cost and can be widely applied to treatment of water polluted by triclosan.

Description

technical field [0001] The invention relates to the field of triclosan wastewater treatment, in particular to an embedded nano-iron / two microbial agent for degrading triclosan and a preparation method thereof. Background technique [0002] Triclosan has a good sterilization and disinfection effect, and has good safety, and even has the effect of promoting human skin metabolism, brightening and moisturizing. Since it was used in soap production in the 1970s, the application scope of triclosan has gradually expanded, and it has been widely used in the production process of personal care products and pharmaceuticals, such as detergents, deodorants, cosmetics, disinfection equipment, and Disinfection and sterilization of textiles before leaving the factory, etc. Triclosan is a polar hydrophobic organic matter, which is easy to deposit in solid phase substances such as soil and bottom mud. The lipophilicity of hydrophobic substances makes it easy to accumulate in organisms, whi...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C12N11/14C12N11/08C12N11/04C12R1/38C12R1/40
CPCC12N11/04C12N11/08C12N11/14
Inventor 陈元彩张君亚黎良浩
Owner SOUTH CHINA UNIV OF TECH