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Preparation method of photo-anode, photo-anode and dye-sensitized solar cell

A photoanode and conductive glass technology, applied in the field of solar cell manufacturing, can solve the problems of poor electron transmission characteristics, light scattering ability, and low specific surface area

Active Publication Date: 2016-09-07
XIDIAN UNIV
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Problems solved by technology

[0006] In view of this, the present application provides a method for preparing a photoanode, a photoanode and a dye-sensitized solar cell, so as to solve the technical problems that the existing dye-sensitized solar cells have poor electron transport characteristics and light scattering ability and a low specific surface area

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  • Preparation method of photo-anode, photo-anode and dye-sensitized solar cell
  • Preparation method of photo-anode, photo-anode and dye-sensitized solar cell

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preparation example Construction

[0019] figure 1 A kind of preparation method of photoanode provided for the embodiment of the present invention, such as figure 1 shown, including:

[0020] S101. Add deionized water and dilute hydrochloric acid into the first hydrothermal reaction kettle and stir, and slowly add titanium isopropoxide dropwise to obtain a first mixed solution, and stir.

[0021] Wherein, the volume of the deionized water is 30 mL, the volume of the dilute hydrochloric acid is 30 mL, the concentration of the dilute hydrochloric acid is 36.5%-38%, and the volume of the titanium isopropoxide is 0.5 mL-0.9 mL.

[0022] S102. Put the FTO conductive glass into the first mixed solution, conduct a hydrothermal reaction at 180°C-210°C for 2-6 hours, take out the FTO conductive glass after cooling down to room temperature naturally, rinse it repeatedly with deionized water, and dry it.

[0023] S103 , sintering the dried FTO conductive glass, and naturally cooling down to room temperature to obtain a ...

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Abstract

The invention provides a preparation method of a photo-anode, the photo-anode and a dye-sensitized solar cell. The preparation method comprises the steps of adding de-ionized water and diluted hydrochloric acid in a first hydrothermal reaction kettle and dripping titanium isopropylate slowly to obtain a first mixed solution; placing FTO (Fluorine-doped Tin Oxide) conducting glass into the first mixed solution for hydrothermal reaction; cooling the first mixed solution to a room temperature and then taking out the FTO conducting glass; sintering the dried FTO conducting glass and cooling the sintered FTO conducting glass to the room temperature so as to obtain a first photo-anode; adding an ethylene glycol solution into a second hydrothermal reaction kettle, adding tetrabutyl titanate into the ethylene glycol solution, adding hydrofluoric acid and acetic acid after mixing, and mixing to obtain a second mixed solution; and adding the first photo-anode into the second mixed solution for hydrothermal reaction, cooling the second mixed solution to the room temperature and then washing the FTO conducting glass with the de-ionized water and drying the FTO conducting glass to obtain a second photo-anode. The technical problems of relatively poor electronic transmission characteristic, relatively poor light scattering ability and small specific surface area of an existing dye-sensitized solar cell are solved.

Description

technical field [0001] The present application relates to the field of solar cell manufacturing, in particular to a method for preparing a photoanode, a photoanode and a dye-sensitized solar cell. Background technique [0002] The energy problem is the most important issue restricting the development of the world economy at present. As an inexhaustible, pollution-free and clean natural green energy, solar energy has become one of the most promising energy sources. At present, the most widely researched and applied solar cells are mainly silicon-based solar cells, but the cost of raw materials for silicon-based cells is high, the production process is complicated, and the potential for efficiency improvement is limited. The theoretical limit of its photoelectric conversion efficiency is 30%, which limits its civilian use. , there is an urgent need to develop low-cost solar cells. [0003] 1991 Swiss Scholar et al. published an article in Nature, and proposed a new type of ...

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Application Information

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IPC IPC(8): H01G9/04H01G9/042H01G9/20H01M14/00H01L51/44H01L51/48
CPCH01M14/005H01G9/04H01G9/042H01G9/2068H10K71/60H10K30/81Y02E10/542Y02E10/549
Inventor 程鹏飞王莹麟卢革宇张华余航苏子生孙鹏
Owner XIDIAN UNIV
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