Synthesis method of furfuryl alcohol, and porous nanometer silicon carbide supported platinum catalyst
A nano-silicon carbide and synthesis method technology, applied in the direction of physical/chemical process catalysts, chemical instruments and methods, organic chemistry, etc., can solve rare problems and achieve the goals of reducing energy consumption, high conversion rate, and reducing production costs Effect
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Embodiment 1
[0048] Example 1 Preparation of Porous Nano-Silicon Carbide Supported Platinum Catalyst 3Pt / SiC
[0049] (a), drop the aqueous solution of chloroplatinic acid in the porous nano-silicon carbide SiC carrier, the weight ratio of its metal platinum and the carrier is 1:32, after ultrasonic, stirring 5 hours, the solvent is naturally dried, then in an oven for 80 Dry at 100°C for 14 hours to obtain a porous nano-silicon carbide supported platinum catalyst precursor;
[0050] (b) Calcining the above catalyst precursor at 200° C. for 4 hours under nitrogen atmosphere.
[0051] (c) Reducing the calcined catalyst precursor at 500° C. for 3 hours in an atmosphere of 99.999% high-purity hydrogen to obtain a porous nano-silicon carbide-supported platinum catalyst 3Pt / SiC.
[0052] The porous nano-silicon carbide material and its large-angle X-ray diffraction as a carrier-supported platinum catalyst 3Pt / SiC are shown in figure 1 ,From figure 1 It can be found that the 2θ is at 35.6°, 6...
Embodiment 2
[0053] Example 2 Preparation of Porous Nano-Silicon Carbide Supported Platinum Catalyst Pt / SiC
[0054] The operating steps and conditions are the same as in Example 1, except that the weight ratio of metal platinum to the carrier is 1:99. The prepared catalyst is Pt / SiC, a platinum catalyst supported on porous nano-silicon carbide.
Embodiment 3
[0055] Example 3 Preparation of Porous Nano-Silicon Carbide Supported Platinum Catalyst 5Pt / SiC
[0056] The operation steps and conditions are the same as in Example 1, except that the weight ratio of metal platinum to the carrier is 1:19. The number of the prepared catalyst is 5Pt / SiC.
[0057] Table 1 Parameters of porous nano-silicon carbide supported platinum catalyst
[0058]
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