Preparation method of environment-friendly coal mine dust reducing agent
A kind of dust suppressant, environment-friendly technology, applied in the field of preparation of environment-friendly coal mine dust suppressant, can solve the problems of poor wettability, secondary pollution, increase dust agglomeration ability, etc., and achieve the effect of low cost and easy operation
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example 1
[0018] According to the volume ratio of 2:3, take egg yolk and calcium chloride solution with a mass fraction of 10% and put it into an ultrasonic oscillator, vibrate at 32kHz for 6min, then add absolute ethanol with 1 times the volume of egg yolk, and put it in a water bath at 45°C In the medium, after preheating for 38 minutes, add 1.3% neutral protease of egg yolk quality, and stir the enzymolysis at 130r / min for 4h; For the supernatant, according to the material-to-liquid ratio of 1:3, take the starch and the supernatant and put them in a microwave oven, heat them at 300W for 20 minutes, then take them out and put them in a rotary evaporator, remove the ethanol solution by rotary evaporation at 80°C, and collect the residue; In parts by weight, take 26 parts of the above-mentioned residue, 36 parts of hydroxymethylcellulose, 15 parts of 20% hydrogen peroxide solution, 3 parts of thiourea and 1 part of formaldehyde. Stir the cellulose evenly, put it into the reaction kettle...
example 2
[0021]According to the volume ratio of 2:3, take egg yolk and calcium chloride solution with a mass fraction of 10% and put it into an ultrasonic oscillator, vibrate at 32kHz for 12min, then add absolute ethanol twice the volume of egg yolk, and put it in a 45°C water bath After preheating for 45 minutes, add 1.6% neutral protease of egg yolk mass, and stir the enzymolysis at 130r / min for 6h; For the supernatant, according to the material-to-liquid ratio of 1:5, take the starch and the supernatant and put them in a microwave oven, heat them at 400W for 30 minutes, then take them out and put them in a rotary evaporator, remove the ethanol solution by rotary evaporation at 80°C, and collect the residue; In parts by weight, take 32 parts of the above-mentioned residue, 34 parts of hydroxymethyl cellulose, 10 parts of 20% hydrogen peroxide solution, 3 parts of thiourea and 1 part of formaldehyde. Stir the cellulose evenly, put it into the reactor after standing at -5°C for 12 minu...
example 3
[0024] According to the volume ratio of 2:3, take egg yolk and calcium chloride solution with a mass fraction of 10% and put them into an ultrasonic oscillator, vibrate at 32kHz for 10min, then add absolute ethanol 1.5 times the volume of egg yolk, and put it in a water bath at 45°C After preheating for 41 minutes, add 1.5% neutral protease of egg yolk mass, and stir the enzymolysis at 130r / min for 5h; For the supernatant, according to the material-to-liquid ratio of 1:4, take the starch and the supernatant and put them in a microwave oven, heat them at 350W for 25 minutes, then take them out and put them in a rotary evaporator, remove the ethanol solution by rotary evaporation at 80°C, and collect the residue; In parts by weight, take 28 parts of the above-mentioned residue, 35 parts of hydroxymethyl cellulose, 12 parts of 20% hydrogen peroxide solution, 5 parts of thiourea and 2 parts of formaldehyde. Stir the cellulose evenly, put it into the reactor after standing at -8°C ...
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