High-stability coating material for hot-blast stove and preparation method thereof
A high-stability, hot-blast stove technology, used in anti-corrosion coatings, fire-retardant coatings, coatings, etc., can solve problems such as cracking, falling off, and affecting the service life of hot-blast stoves
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[0013] The invention provides a kind of preparation method of the high stability coating that is used for hot blast furnace, comprises:
[0014] 1) Soaking river mud in acid solution, then filtering to get filter cake to obtain modified river mud;
[0015] 2) Disperse silica gel, sodium zirconate, rare earth oxide and modified river mud in an organic solvent under ultrasonic conditions, and then filter the filter cake to obtain the activated product;
[0016] 3) Organic silicon, acrylonitrile-butadiene-styrene copolymer, maleic anhydride, organic solvent, carbon fiber, attapulgite, cyclodextrin and activator are subjected to contact reaction under high pressure and airtight conditions to Produces highly stable coatings for hot blast stoves.
[0017] In step 1) of the present invention, the specification of the filter paper used for filtering can be selected in a wide range, but in order to improve the high temperature resistance and corrosion resistance of the high stability ...
Embodiment 1
[0030] 1) Soak the river mud in an acid solution with a pH of 4 (the weight ratio of the river mud to the acid solution is 100:400), and then filter through filter paper with a pore size of 40 μm to obtain a modified river mud;
[0031] 2) Mix silica gel, sodium zirconate, rare earth oxide (cerium oxide), modified river mud and organic solvent (acetophenone) in a weight ratio of 100:15:26:55:500, and heat Disperse for 6h at a frequency of 50MHz, then filter the filter cake to obtain the activated product;
[0032] 3) Silicone (methyltriethoxysilane), acrylonitrile-butadiene-styrene copolymer, maleic anhydride, organic solvent (cyclohexanone), carbon fiber, attapulgite, cyclodextrin Mix with the activator according to the weight ratio of 100:40:65:350:8:19:10:34, and conduct a contact reaction at 80°C, 1.8MPa and airtight conditions for 8 hours to obtain a highly stable Sexual coating A1.
Embodiment 2
[0034] 1) Soak the river mud in an acid solution with a pH of 3 (the weight ratio of the river mud to the acid solution is 100:300), and then filter through a filter paper with a pore size of 30 μm to obtain a filter cake to obtain a modified river mud;
[0035] 2) Mix silica gel, sodium zirconate, rare earth oxide (praseodymium oxide), modified river mud and organic solvent (acetophenone) in a weight ratio of 100:11:21:40:400, and heat the Disperse for 5h at a frequency of 40MHz, then filter the filter cake to obtain the activated product;
[0036] 3) Silicone (dimethyldiethoxysilane), acrylonitrile-butadiene-styrene copolymer, maleic anhydride, organic solvent (tert-amyl alcohol), carbon fiber, attapulgite, cyclopaste The essence and the activator are mixed according to the weight ratio of 100:35:60:250:5:15:7:30, and the contact reaction is carried out at 75°C, 1.5MPa and airtight conditions for 6 hours to obtain high Stabilization paint A2.
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