High-temperature resistant paint for hot-blast stoves and preparation method of high-temperature resistant paint
A technology for high temperature resistant coatings and hot blast stoves, which is applied in the direction of anti-corrosion coatings, fireproof coatings, coatings, etc., and can solve problems such as shedding, affecting the service life of hot blast stoves, and cracking
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[0013] The invention provides a method for preparing a high temperature resistant coating for a hot blast stove, comprising:
[0014] 1) Soaking river mud in acid solution, then filtering to get filter cake to obtain modified river mud;
[0015] 2) Disperse silica gel, sodium zirconate, rare earth oxide and modified river mud in an organic solvent under ultrasonic conditions, and then filter the filter cake to obtain the activated product;
[0016] 3) Contact reaction of organosilicon, acrylonitrile-butadiene-styrene copolymer, maleic anhydride, organic solvent, carbon fiber, diatomaceous earth, cyclodextrin and activator under high pressure and airtight conditions to obtain High temperature resistant coatings for hot blast stoves.
[0017] In step 1) of the present invention, the specifications of the filter paper used for filtering can be selected in a wide range, but in order to improve the high temperature resistance and corrosion resistance of the high temperature resist...
Embodiment 1
[0030] 1) Soak the river mud in an acid solution with a pH of 4 (the weight ratio of the river mud to the acid solution is 100:400), and then filter through filter paper with a pore size of 40 μm to obtain a modified river mud;
[0031] 2) Mix silica gel, sodium zirconate, rare earth oxide (cerium oxide), modified river mud and organic solvent (acetophenone) in a weight ratio of 100:15:25:47:550, and heat Disperse for 7 hours at a frequency of 50 MHz, then filter the filter cake to obtain the activated product;
[0032] 3) Silicone (methyltriethoxysilane), acrylonitrile-butadiene-styrene copolymer, maleic anhydride, organic solvent (cyclohexanone), carbon fiber, diatomaceous earth, cyclodextrin and activated The materials were mixed according to the weight ratio of 100:40:60:300:8:29:10:25, and the contact reaction was carried out at 80°C, 1.8MPa and airtight conditions for 8 hours to prepare the high temperature resistant coating A1 for hot blast stove .
Embodiment 2
[0034] 1) Soak the river mud in an acid solution with a pH of 3 (the weight ratio of the river mud to the acid solution is 100:300), and then filter through a filter paper with a pore size of 30 μm to obtain a filter cake to obtain a modified river mud;
[0035] 2) Mix silica gel, sodium zirconate, rare earth oxide (praseodymium oxide), modified river mud and organic solvent (acetophenone) in a weight ratio of 100:11:21:40:400, and heat the Disperse for 5h at a frequency of 40MHz, then filter the filter cake to obtain the activated product;
[0036] 3) Silicone (dimethyldiethoxysilane), acrylonitrile-butadiene-styrene copolymer, maleic anhydride, organic solvent (tert-amyl alcohol), carbon fiber, diatomaceous earth, cyclodextrin and The activators are mixed according to the weight ratio of 100:35:55:250:5:23:7:19, and the contact reaction is carried out at 75°C, 1.5MPa and airtight conditions for 6 hours to prepare a high temperature resistant coating for hot blast stoves A2....
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