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Water-blown inorganic hybrid melamine polyurethane rigid foam material and manufacturing method thereof

A technology of hybrid melamine polyurethane and hybrid melamine, which is applied in the field of water-foamed polyurethane rigid foam materials and its manufacturing, can solve the problems of high viscosity, high thermal conductivity, and poor fluidity of the system, and achieve high temperature resistance and flame retardancy Improvement of performance and improvement of flame retardant performance

Active Publication Date: 2016-12-21
CHANGZHOU JUMBO ENERGY SAVING TECH CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0006] However, ordinary all-water foamed rigid polyurethane foam has many shortcomings, such as too high viscosity, poor fluidity, uneven foaming, resulting in coarse cells, large thermal conductivity, and brittle foam, etc.

Method used

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  • Water-blown inorganic hybrid melamine polyurethane rigid foam material and manufacturing method thereof
  • Water-blown inorganic hybrid melamine polyurethane rigid foam material and manufacturing method thereof
  • Water-blown inorganic hybrid melamine polyurethane rigid foam material and manufacturing method thereof

Examples

Experimental program
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Effect test

Embodiment 1

[0045] Water foaming inorganic hybrid melamine polyurethane rigid foam material, the material is a rigid foam material formed by foaming inorganic hybrid melamine polyurethane polyether and polymerized isocyanate, inorganic hybrid melamine polyurethane polyether, in parts by weight, The formula is as follows:

[0046]

[0047] The emulsifier is hard foam silicone oil.

[0048] The composite catalyst is potassium acetate and pentamethyldiethylenetriamine.

[0049] The flame retardant is phosphoric acid ester, the phosphoric acid ester is tris(1-chloro-2-propyl) phosphate, and the viscosity of the phosphoric acid ester is 290 Pa·s.

[0050] Inorganic hybrid melamine resin polyol is specifically boron hybrid melamine resin propylene glycol, and its molecular structural formula and preparation method are as follows:

[0051]

[0052] Raw material ratio:

[0053]

[0054]

[0055] (1) etherification reaction

[0056] Add hexamethylol melamine and methanol into the rea...

Embodiment 2

[0073] Water foaming inorganic hybrid melamine polyurethane rigid foam material is a rigid foam material formed by foaming inorganic hybrid melamine polyurethane combined with polyether and polymerized isocyanate, characterized in that:

[0074] Water foaming inorganic hybrid melamine polyurethane rigid foam material is a rigid foam material formed by foaming inorganic hybrid melamine polyurethane combined with polyether and polymerized isocyanate, characterized in that:

[0075] Described inorganic hybrid melamine polyurethane combination polyether, by weight ratio, formula is as follows:

[0076]

[0077] The emulsifier is hard foam silicone oil.

[0078] The composite catalyst is pentamethyldiethylenetriamine, 1,3,5-tris(dimethylaminopropyl)hexahydrotriazine, trimethyl-N-2 hydroxypropyl hexanoic acid and dilauric acid di Butyl tin.

[0079] The flame retardant is phosphoric acid ester, the phosphoric acid ester is tris(2,3-dichloropropyl) phosphate, and the viscosity o...

Embodiment 3

[0103] Water foaming inorganic hybrid melamine polyurethane rigid foam material is a rigid foam material formed by foaming inorganic hybrid melamine polyurethane combined with polyether and polymerized isocyanate, characterized in that:

[0104] Water foaming inorganic hybrid melamine polyurethane rigid foam material is a rigid foam material formed by foaming inorganic hybrid melamine polyurethane combined with polyether and polymerized isocyanate, characterized in that:

[0105] Described inorganic hybrid melamine polyurethane combination polyether, by weight ratio, formula is as follows:

[0106]

[0107] The emulsifier is hard foam silicone oil.

[0108] The composite catalyst is 1,3,5-tris(dimethylaminopropyl)hexahydrotriazine, triethylenediamine and N,N-dimethylaniline.

[0109] The flame retardant is phosphoric acid ester, and the phosphoric acid ester is tris(1-chloro-2-propyl) phosphate and tris(2,3-dichloropropyl) phosphate, and the viscosity of the phosphoric aci...

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Abstract

The invention provides a water-blown inorganic hybrid melamine polyurethane rigid foam material and a manufacturing method thereof, belonging to the fields of production of flame-retardant polyurethane energy-saving materials and building energy-saving technology. The manufacturing method comprises the following steps: with high-temperature-resistant inorganic hybrid melamine resin polyol or inorganic hybrid polyol etherified melamine resin, an emulsifier, a composite catalyst, a phosphate fire retardant, a foaming agent, and water or soluble glass as mainly raw materials, carrying out dispersion under stirring to separately prepare combined polyether; and then subjecting the prepared combined polyether and isocyanate MDI to foaming on a panel machine, a spray coater and a casting machine so as to prepare the environment-friendly water-blown inorganic hybrid melamine polyurethane rigid foam material with B1-grade flame retardation performance. The material provided by the invention is free of lower-boiling-point hydrocarbon compound chlorofluorocarbon and hydrochloroflurocarbon compounds, undergoes foaming in virtue of water, does not destroy an ozone layer nor produce greenhouse effect and is environment friendly; the flame resistance of the material is improved by at least 20%; and the material has excellent flame resistance while guaranteeing physical properties and has an oxygen index of more than 30%.

Description

technical field [0001] The invention belongs to the technical fields of flame-retardant polyurethane energy-saving material production and building energy conservation, and in particular relates to water-foamed polyurethane hard foam material and a manufacturing method thereof. Background technique [0002] my country is a large country with complex climate characteristics, such as the severe cold in the Northeast and the middle reaches of the Yangtze River in hot summer and cold in winter, which makes the energy consumption of building materials in my country very large. Winter warming in the northern region accounts for 27.3% of the country's total energy consumption. However, due to the problems of materials, technology and workmanship, the heating energy consumption per unit area of ​​traditional buildings in my country is 2-3 times that of developed countries with similar climate conditions in the world. The "Medium and Long-term Special Plan for Energy Conservation" p...

Claims

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Application Information

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IPC IPC(8): C08G18/32C08K5/521C08J9/08C08G101/00
CPCC08G18/3897C08J9/08C08J2203/02C08J2375/12C08K5/521C08G2110/0025C08G2110/0083C08G18/32
Inventor 王洪波李强
Owner CHANGZHOU JUMBO ENERGY SAVING TECH CO LTD
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