Ionic palladium activation solution for manufacturing conductor lines on ceramics and preparation method thereof
A conductor line, palladium activation technology, applied in the field of ionic palladium activation solution and its preparation, can solve the problems of uneven conductor line thickness, uneven line, poor line integrity, etc., to achieve good adhesion and reliability, electrical performance testing Stable, good adhesion effect
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Embodiment 1
[0036] Configuration of palladium ion activation solution and working solution
[0037] (1) First, dissolve 3g of palladium sulfate in 100ml of sulfuric acid with a volume fraction of 50%, stir at 50°C at a speed of 200r / min for 1h, add deionized water to 800ml, and then add 10-100ml of methyl silane polymer carrier solution , after stirring at 50°C at 10r / min for 30min, add 1-100ml of surfactant naphthalenesulfonate solution, dilute to 1L with deionized water, stir at 50°C at 100r / min for 2-4h, then let stand for 48 The ionic palladium activation solution can be obtained within hours.
[0038] (2) Configuration of the working solution: add 200ml of deionized water to a 1L beaker, add 50ml of analytically pure sulfuric acid, stir and cool to 20°C, add 20ml of the ionic palladium activation solution prepared in step (1), and use deionized water Replenish to 1L, heat to 30°C, stir for 10 minutes, and then use.
Embodiment 2
[0040] Configuration of palladium ion activation solution and working solution
[0041] (1) First, 3g of palladium sulfate is dissolved in 100ml, 50% volume fraction of acetic acid, after stirring for 1h at 50°C with a rotating speed of 200r / min, add deionized water to 800ml, then add 10-100ml gum arabic polymer carrier solution, After stirring at 50°C at 10r / min for 30min, add 1-100ml of surfactant naphthalenesulfonate solution, dilute to 1L with deionized water, stir at 50°C at 100r / min for 2-4h, then let stand for 48 hours That is, the ionic palladium activation solution is obtained.
[0042] (2) Configuration of the working solution: add 200ml of deionized water to a 1L beaker, add 50ml of analytically pure sulfuric acid, stir and cool to 20°C, add 20ml of the ionic palladium activation solution prepared in step (1), and use deionized water Replenish to 1L, heat to 30°C, stir for 10 minutes, and then use.
Embodiment 3
[0044] Configuration of palladium ion activation solution and working solution
[0045] (1) First, dissolve 4g of palladium chloride in 100ml of succinic acid with a volume fraction of 50%, stir at 50°C at 200r / min for 1h, add deionized water to 800ml, and then add 10-100ml of carboxymethyl cellulose Sodium polymer carrier solution, stir at 50°C at 10r / min for 30min, add 1-100ml of surfactant sodium dodecylsulfonate solution, dilute to 1L with deionized water, stir at 50°C at 100r / min After 2-4 hours, let it stand for 48 hours to obtain the ionic palladium activation solution.
[0046] (2) Configuration of the working solution: add 200ml of deionized water to a 1L beaker, add 50ml of analytically pure phosphoric acid, stir and cool to 20°C, add 20ml of the ionic palladium activation solution prepared in step (1), and use deionized water Replenish to 1L, heat to 30°C, stir for 10 minutes, and then use.
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