Photocatalysis material with nano TiO2 loaded on kieselguhr white carbon black used as carrier and preparation method of photocatalysis material
A technology of photocatalytic material and earth white carbon black, which is applied in the field of photocatalytic materials, can solve the problems that the photocatalytic performance needs to be further improved, the titanium dioxide loading is not high, and the preparation cost is high, and achieves small grain size, low cost, and easy operation. simple effect
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[0021] The above mentioned diatomaceous earth white carbon black as carrier loaded nano TiO 2 The preparation method of photocatalytic material, step is as follows:
[0022] Step 1. Stir and mix water and diatomite silica according to the mass ratio (28-32): 1, and adjust the pH value to 1-2 with hydrochloric acid to obtain a diatomite silica slurry;
[0023] Among them, the concentration of diatomite silica slurry and TiO 2 The load is the same, which is related to product performance and cost; if the mass ratio of water and diatomite silica is less than 28:1, the concentration of diatomite silica slurry increases, and the same TiO 2 In the case of loading, TiO per unit carrier surface 2 Too low, and under the action of electrostatic attraction, the carrier will be agglomerated and the specific surface area will be reduced, which is not conducive to TiO 2 If the mass ratio of water and diatomite silica is greater than 32:1, the concentration of diatomite silica slurry will...
Embodiment 1
[0028] Nano-TiO loaded on diatomite silica as carrier 2 Photocatalytic material with a whiteness of 80, composed of diatomite silica and nano-titanium dioxide supported on diatomite silica; the silica content of diatomite silica is 98.55%, and the particle size is 15 ~40um, loss on ignition is 2.21%, specific surface area is 520m 2 / g, the pore volume is 0.63ml / g; the loading capacity of nano-titanium dioxide is 38%, and the grain size is 12.65nm.
[0029] Nano-TiO loaded on diatomite silica as carrier 2 Preparation method of photocatalytic material:
[0030] Step 1. Stir and mix water and diatomite silica according to a mass ratio of 30:1, and adjust the pH value to 1.5 with hydrochloric acid to obtain a diatomite silica slurry;
[0031] Step 2. When the temperature of diatomite silica slurry drops to -5°C, add titanium tetrachloride solution and ammonium sulfate solution, raise the temperature to 50°C, keep it warm for 1.2h, then add ammonium carbonate solution to adjust ...
Embodiment 2
[0034] Nano-TiO loaded on diatomite silica as carrier2 Photocatalytic material with a whiteness of 84, composed of diatomite silica and nano-titanium dioxide supported on diatomite silica; the silica content of diatomite silica is 98.79%, and the particle size is 15 ~40um, loss on ignition is 2.2%, specific surface area is 516m 2 / g, the pore volume is 0.68ml / g; the loading capacity of nano-titanium dioxide is 40%, and the grain size is 13.2nm.
[0035] Nano-TiO loaded on diatomite silica as carrier 2 Preparation method of photocatalytic material:
[0036] Step 1. Stir and mix water and diatomite silica according to a mass ratio of 28:1, and adjust the pH value to 1 with hydrochloric acid to obtain a diatomite silica slurry;
[0037] Step 2. When the temperature of the diatomite silica slurry drops to -4°C, add titanium tetrachloride solution and ammonium sulfate solution, raise the temperature to 55°C, keep it warm for 1 hour, then add ammonium carbonate solution to adjust ...
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