Method for preparing semen cassiae microcapsule particles

A technology for cassia seeds and granules is applied in the field of preparing cassia seed microcapsule particles, which can solve the problems of quality decline, oxidative degradation, nutrient loss, etc., and achieve the effects of improving water solubility, good dispersibility, and improving compactness.

Inactive Publication Date: 2017-03-15
广西放心源生物科技有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, cassia seed dry powder is not protected by other media, and it is prone to oxidative degradation under the action of light, high temperature and oxygen, resulting in loss of nutrition and quality decline.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0025] A method for preparing cassia seed microcapsules, comprising the following steps:

[0026] (1) Preparation of core material: crush 100 kg of dried cassia seeds, add 500 kg of ethanol with a mass concentration of 95% to dissolve, then add 12 kg of Tween 80 emulsifier, stir evenly, and obtain a core material solution;

[0027] (2) Preparation of wall material: dissolving gelatin and glyceryl monostearate in water to obtain a wall material solution, wherein the mass ratio of gelatin to glyceryl monostearate to water is 12:8:100;

[0028] (3) Ultrasonic homogenization: Add the above-mentioned core material solution and wall material solution into an ultrasonic homogenizer at a mass ratio of 1:5, and homogenize for 30 minutes at a power of 200W and a temperature of 50°C;

[0029] (4) Microwave drying: Microwave-dry the slurry obtained in step (3) at a temperature of 60°C to obtain dry powder with a water content of 7%, cool to room temperature, and pack to obtain cassia seed...

Embodiment 2

[0031] A method for preparing cassia seed microcapsules, comprising the following steps:

[0032] (1) Preparation of core material: crush 100 kg of dried cassia seeds, add 500 kg of ethanol with a mass concentration of 95% to dissolve, then add 10 kg of Tween 80 emulsifier, stir evenly, and obtain a core material solution;

[0033] (2) Preparation of wall material: dissolving gelatin and glyceryl monostearate in water to obtain a wall material solution, wherein the mass ratio of gelatin to glyceryl monostearate to water is 10:10:100;

[0034] (3) Ultrasonic homogenization: Add the above-mentioned core material solution and wall material solution into an ultrasonic homogenizer at a mass ratio of 1:4, and homogenize for 20 minutes at a power of 250W and a temperature of 60°C;

[0035] (4) Microwave drying: Microwave-dry the slurry obtained in step (3) at a temperature of 70°C to obtain a dry powder with a water content of 6%, which is cooled to room temperature and packaged to o...

Embodiment 3

[0037] A method for preparing cassia seed microcapsules, comprising the following steps:

[0038] (1) Preparation of core material: crush 100 kg of dried cassia seeds, add 600 kg of ethanol with a mass concentration of 90% to dissolve, then add 15 kg of Tween 60 emulsifier, stir evenly, and obtain a core material solution;

[0039] (2) Preparation of wall material: dissolving gelatin and glyceryl monostearate in water to obtain a wall material solution, wherein the mass ratio of gelatin to glyceryl monostearate to water is 15:8:100;

[0040] (3) Ultrasonic homogenization: Add the above-mentioned core material solution and wall material solution into an ultrasonic homogenizer at a mass ratio of 1:6, and homogenize for 25 minutes at a power of 250W and a temperature of 50°C;

[0041] (4) Microwave drying: Microwave-dry the slurry obtained in step (3) at a temperature of 50°C to obtain dry powder with a water content of 8%, cool to room temperature, and pack to obtain cassia seed...

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PUM

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Abstract

The invention discloses a method for preparing semen cassiae microcapsule particles. The method comprises the steps that dry semen cassiae is crushed, ethyl alcohol is added for dissolving Tween emulsifier accounting for 10%-15% of the mass of semen cassiae is added, stirring is conducted to be uniform, and a core material solution is obtained; gelatin and glyceryl monostearate are dissolved into water, and a wall material solution is obtained, wherein the mass ratio of gelatin to glyceryl monostearate to water is (10-15):(5-10):100; the core material and the wall material solution are added into an ultrasonic homogenizer to be subjected to homogenization treatment for 20-30 min according to the mass ratio of 1:(4-6); obtained slurry is subjected to microwave drying, dry powder with the water content being 6%-8% is obtained, cooling is conducted to room temperature, packaging is conducted, and the semen cassiae microcapsule particles are obtained. According to the method, the stability of semen cassiae can be significantly improved, the storage period can be obviously prolonged, full-nutrients and active ingredients of raw semen cassiae powder can be well preserved, and technical processing, storage and transport of semen cassiae are convenient.

Description

technical field [0001] The invention relates to the technical field of Chinese herbal medicine processing, in particular to a method for preparing cassia seed microcapsule particles. Background technique [0002] Cassia, also known as horseshoe cassia, blunt leaf cassia, false mung bean, grass cassia, is the dry mature seed of leguminous plant cassia or small cassia. In addition to carbohydrates, proteins, and fats, cassia seeds also contain steroidal compounds, chrysophanol, emodin, etc., as well as essential trace elements such as iron, zinc, manganese, copper, nickel, cobalt, and molybdenum. Cassia seed has the functions of clearing liver-fire, dispelling rheumatism, benefiting kidney and improving eyesight, etc. Drinking cassia seed tea regularly can make blood pressure normal, defecate unobstructed, and prevent old eyes from blurring. Clinical experiments have proved that drinking cassia seed tea can clear the liver and improve eyesight, prevent blurred vision, lower b...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): A61K9/50A61K47/42A61K47/14A61K36/482
CPCA61K9/5057A61K9/5015A61K36/482
Inventor 凌雪木
Owner 广西放心源生物科技有限公司
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