Non-chloride ion potassium salt water-locking agent for oil well cement, preparation method and application thereof

A technology of oil well cement and ionic potassium, applied in the direction of chemical instruments and methods, drilling compositions, etc., can solve the problems of long waiting setting time, slow hydration rate of cement slurry, long initial setting time, etc., to achieve accelerated setting and Hardening, promoting formation and development, and improving the effect of impermeability

Active Publication Date: 2017-03-22
BC P INC CHINA NAT PETROLEUM CORP +1
View PDF4 Cites 2 Cited by
  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0002] At present, most wells are cemented with raw slurry. The cement for raw slurry cementing enters the ash mixing funnel from the ash lowering device. The water is jetted from the nozzle and fully mixed with the cement to form cement slurry. The slurry mixing speed is determined by the amount of water sprayed from the nozzle. Determined by the amount of ash in the funnel, the initial setting time is long, the compressive strength is low, the cement gel strength develops slowly, the permeability is high, the gel weight loss of the cement slurry cannot be compensated, the cementing quality cannot be guaranteed, and the cementing quality rate only about 60%
[0003] Under low temperature conditions, due to the slow hydration rate and long waiting time of cement slurry, it is easy to cause oil, gas and water immersion, resulting in poor cementing quality
At present, the most commonly used oil well cement water-locking agent for low-temperature shallow well cementing in oil fields is chloride, but due to the addition of chloride, the cement slurry thickens seriously, heat is released rapidly in the cement slurry, and even premature solidification occurs. The pipe is highly corrosive, which leads to a great degree of limitation in its use

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more

Image

Smart Image Click on the blue labels to locate them in the text.
Viewing Examples
Smart Image
  • Non-chloride ion potassium salt water-locking agent for oil well cement, preparation method and application thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0018] In order to solve the problem that the existing cement slurry has a long waiting time, which can easily cause oil, gas, and water flooding, resulting in poor cementing quality and strong corrosion to the casing, this embodiment provides a non-chloride ion cement for oil well cement. The potassium salt water-locking agent is composed of the following materials in mass percentage: 40-60% potassium salt, 10-30% alkali, and 20-40% sodium silicate.

[0019] Principle of the present invention:

[0020] Potassium ions in the formula have a coagulation-promoting effect, and the hydration reacts rapidly, providing a skeleton of the cohesion structure for the cement paste, promoting the formation and development of cement hydration products, and accelerating the coagulation and hardening of cement; the sodium ions in sodium silicate React with cement to form colloid, which can fill the pores between cement, make the structure of cement stone compact, high density, and improve imp...

Embodiment 2

[0023] On the basis of Example 1, this example provides a non-chloride ion potassium salt water-locking agent for oil well cement, which is composed of the following materials in mass percentage: 40% potassium salt, 30% alkali, 30% sodium silicate %.

[0024] Preparation process: Add 400 Kg of potassium salt, 300 Kg of alkali, and 300 Kg of sodium silicate to a mixer, mix and stir for 40 minutes.

[0025] In this embodiment, the potassium salt is potassium sulfate, and the base is sodium hydroxide. Sodium ions in sodium silicate react with cement to form colloid, which can fill the pores between cement, make the structure of cement stone dense, high density, and improve impermeability.

Embodiment 3

[0027] On the basis of Example 1, this example provides a non-chloride ion potassium salt water-locking agent for oil well cement, which is composed of the following materials in mass percentage: 50% potassium salt, 20% alkali, 30% sodium silicate %.

[0028] Preparation process: Add 500 Kg of potassium salt, 200 Kg of alkali, and 300 Kg of sodium silicate into a mixer, and mix and stir for 30 minutes.

[0029] In this embodiment, the potassium salt is potassium sulfate, and the base is calcium hydroxide.

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to view more

PUM

No PUM Login to view more

Abstract

Belonging to the technical field of oil-gas well cementing additives for the petroleum industry, the invention provides a non-chloride ion potassium salt water-locking agent for oil well cement, a preparation method and application thereof. The non-chloride ion potassium salt water-locking agent is composed of the following materials by mass percentage: 40-60% of a potassium salt, 10-30% of alkali, and 20-40% of sodium silicate, can effectively improve the early strength of cement stone, greatly shortens the well cementing setting waiting time, is free of chlorine ions and other corrosive ions, has no corrosive effect on casing pipes and cement stone, is easy for dry blending, has obvious reinforcing effect on cement slurry, low hydration heat and small influence on the rheological properties of cement slurry, and is conducive to site construction operation.

Description

technical field [0001] The invention belongs to the technical field of oil and gas well cementing additives used in the petroleum industry, and in particular relates to a non-chloride ion potassium salt water-locking agent for oil well cement, a preparation method and application thereof. Background technique [0002] At present, most wells are cemented with raw slurry. The cement for raw slurry cementing enters the ash mixing funnel from the ash lowering device. The water is jetted from the nozzle and fully mixed with the cement to form cement slurry. The slurry mixing speed is determined by the amount of water sprayed from the nozzle. Determined by the amount of ash in the funnel, the initial setting time is long, the compressive strength is low, the cement gel strength develops slowly, the permeability is high, the gel weight loss of the cement slurry cannot be compensated, the cementing quality cannot be guaranteed, and the cementing quality rate Only about 60%. [0003...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to view more

Application Information

Patent Timeline
no application Login to view more
Patent Type & Authority Applications(China)
IPC IPC(8): C04B22/14C04B22/08C09K8/467C04B103/46
CPCC04B40/0039C04B2103/465C09K8/467C04B22/147C04B22/062C04B14/045C04B22/085C04B22/064
Inventor 梅佳明李德伟窦虎清段宏超
Owner BC P INC CHINA NAT PETROLEUM CORP
Who we serve
  • R&D Engineer
  • R&D Manager
  • IP Professional
Why Eureka
  • Industry Leading Data Capabilities
  • Powerful AI technology
  • Patent DNA Extraction
Social media
Try Eureka
PatSnap group products