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Mass spectrometer and pole used for same

A mass spectrometer and pole technology, applied in the field of detection and analysis equipment, can solve the problems of lack of firm connection and fixation of the quadrupole, failure to obtain the pole, and reduced service life, etc., to achieve low secondary ion effect, low cost, and long service life long effect

Active Publication Date: 2017-05-03
NORTHEASTERN UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0012] The quadrupoles are closely attached to the inner wall of the ceramic ring and are evenly distributed. There are ceramic columns between adjacent quadrupoles. Each ceramic column is tangent to the adjacent quadrupole and the inner wall of the ceramic ring. The ceramic columns and quadrupoles are respectively Using the same size, the processing of ceramic rings, ceramic columns, and quadrupole rods has no complicated curved surfaces, so it is easy to process. However, because there are many interactions between multiple parts and the requirements are high, higher processing and assembly requirements are required. , in addition, due to the lack of firm connections between the quadrupole, the ceramic column and the ceramic ring, the service life will be reduced
[0013] In summary, although the current improvement methods have their own advantages, on the whole, it is impossible to obtain a pole that meets the requirements of cost reduction, high precision, and long life at the same time

Method used

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  • Mass spectrometer and pole used for same
  • Mass spectrometer and pole used for same
  • Mass spectrometer and pole used for same

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0048] refer to figure 1 , In this embodiment, a pole for a mass spectrometer is provided. The pole rod for the mass spectrometer includes a pole body and a film layer, and the film layer is formed on the pole body by a vacuum coating process. In this embodiment, the film layer covers the entire outer peripheral surface of the pole body, and the two ends of the pole body are not covered with the film layer. Wherein, the "pole body" is equivalent to the pole in the prior art.

[0049] Vacuum coating technology is to use a certain method under vacuum conditions to coat a thin layer of material different from the base material on the solid surface, or to use the solid itself to generate a thin layer of material different from the base material. Different materials make the base material have many new physical and chemical properties, so vacuum coating technology is also called surface modification technology. The invention breaks through the improvement ideas of the prior art ...

Embodiment 2

[0060] refer to image 3 The difference between this embodiment and Embodiment 1 is that the vacuum coating process is a vacuum evaporation coating process.

[0061] First, the rod body 204 is placed on the substrate frame 203, and the substrate frame 203 rotates at a constant speed during coating, and a substrate heating device 201 is arranged above the substrate frame 203, and the ceramic film material is placed in the evaporation boat 206, and the ceramic film material placed in the image 3 The position of the middle membrane material 205 shows that the coating chamber 202 is pumped to the working pressure, and the ceramic membrane material in the evaporation boat 206 is heated by the evaporation boat heating device 207, so that the evaporated atoms and molecules escape from the surface of the membrane material and directly reach the On the surface of the rod body 204 installed on the substrate frame 203 (the steam flow 209 is indicated by the arrow in the figure), due to...

Embodiment 3

[0064] refer to Figure 4 The difference between this embodiment and Embodiment 1 is that the vacuum coating process is a vacuum sputtering coating process, preferably a magnetron sputtering coating process.

[0065] Specifically, in the coating chamber 303, the rod body is placed on the substrate holder 301, the metal target and the ceramic target are installed on the target position 308, the metal target and the ceramic target are located under the substrate holder 301, and the heating device 302 is used to Heating metal / ceramic targets. Firstly, the ceramic target is facing the substrate frame 301, and the base distance of the target is adjusted to the set distance, and then the coating chamber 303 is pumped by the pumping system 304, and after reaching the background vacuum degree, the working gas is introduced by the pumping system 307 , after reaching the working pressure of 1.0-2.0Pa, turn on the heating power supply 305 and the negative high-voltage power supply 306, ...

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Abstract

The invention relates to a detection analysis device, and particularly to a mass spectrometer and a pole used for the same. The pole comprises a pole body and a film layer; and the film layer is formed on a pole body by adopting a vacuum film plating technology. The vacuum film plating technology has lower cost than the existing complex processing technology. By carrying out film plating processing on the surface of the pole body, the manufacturing deficiency of the pole body can be made up, the pole dimension precision can be improved, the pole is enabled to meet the processing precision requirements such as the cylindricity and the surface roughness, and the pole is enabled to have the characteristics such as good conductivity, good corrosion resistance, good thermal stability, relatively low vacuum air release, relatively low secondary ion effect, difficult surface particle release and pollution resistance. Furthermore, the mass spectrometer using the pole can generate an ideal electric field; and the service lifetime of the pole is prolonged while the detection work is finished; the requirement on the material type of the pole body is reduced, and materials at low cost can be selected. The mass spectrometer comprises the pole, is low in cost, can guarantee generation of the ideal electric field and is long in service lifetime.

Description

technical field [0001] The invention relates to detection and analysis equipment, in particular to a pole rod for a mass spectrometer and a mass spectrometer. Background technique [0002] As an important gas analysis instrument in vacuum measurement and leak detection, quadrupole mass spectrometer has the function of simultaneously analyzing various residual gas components in the space. Therefore, in vacuum leak detection, the quadrupole mass spectrometer can not only perform single-point leak detection on the sealing system filled with different leak-indicating media, but also realize the test of the total leak rate of each sealing system, shortening the time to the maximum extent. Leak detection cycle. [0003] A quadrupole mass spectrometer is mainly composed of three parts: ion source, analyzer and collector. The function of the ion source is to ionize gas molecules, generate positive ions and send them to the analyzer. The analyzer screens the incoming ions and sends...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): H01J49/42H01J49/02
CPCH01J49/02H01J49/4215
Inventor 刘坤孙飞刘晓杰姚文浩邓文宇陈树雷杜广煜巴德纯
Owner NORTHEASTERN UNIV
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