Iron-doped titanium nitride nanotubes as well as preparation method and application of iron-doped titanium nitride nanotubes
An iron-doped, titanium nitride technology, used in chemical instruments and methods, nitrogen compounds, nanotechnology, etc., to achieve the effects of good electrical conductivity and electrochemical stability, safe operation, and simple operation
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Image
Examples
Embodiment 1
[0031] Weigh 0.0203g of ferric chloride and 2.000g of titanyl sulfate and mix them, add them in turn to an autoclave with a polytetrafluoroethylene liner (100mL), then add 15mL of butanediol, 15mL of butyl ether and 30mL of absolute ethanol . Then put the polytetrafluoroethylene lining in the ultrasonic instrument for 30 minutes, and then stir for another 30 minutes. After the stirring, put the polytetrafluoroethylene lining with the reactants into the reaction kettle, and react at 120 ° C for 16 hours; After the reaction kettle is naturally cooled to room temperature, it is filtered, washed with distilled water and absolute ethanol in turn, and then dried in a 60°C oven for 15 hours; then placed in a muffle furnace for calcination at 300°C for 5 hours, and finally in a tube furnace Calcined at 700 °C for 5 h to obtain iron-doped titanium nitride nanotubes.
[0032] figure 1 It is the XRD pattern of the iron-doped titanium nitride nanotube prepared in Example 1. Among them,...
Embodiment 2
[0036] Weigh 0.2028g of ferric chloride and 2.000g of titanyl sulfate and mix them; add them in turn to an autoclave with a polytetrafluoroethylene liner (100mL), then add 15mL of butanediol, 15mL of butyl ether and 30mL of absolute ethanol . First put the polytetrafluoroethylene liner with the reactants in the ultrasonic instrument for 30min, then stir for 30min. ℃ for 12 hours; the reaction kettle was naturally cooled to room temperature, then filtered, washed with distilled water and absolute ethanol in turn, and then dried in an oven at 70 ℃ for 14 hours; then calcined in a muffle furnace at 400 ℃ for 4 hours, and finally Calcining at 750° C. for 3 h in a tube furnace to obtain iron-doped titanium nitride nanotubes.
[0037] Figure 4 This is the SEM image of the iron-doped titanium nitride nanotubes obtained in Example 2. The obtained iron-doped titanium nitride nanotubes have an average diameter of 50-200 nm and are composed of iron-doped titanium nitride nanoparticles...
Embodiment 3
[0039] Weigh 0.2028g of ferric chloride and 2.000g of titanyl sulfate and mix them into a polytetrafluoroethylene-lined (100mL) autoclave, then add 15mL of butanediol, 15mL of butyl ether and 30mL of absolute ethanol. First, put the polytetrafluoroethylene lining added with the reactant in the ultrasonic instrument for 30 minutes, and then stir for 30 minutes. React at ℃ for 10 hours; after the reactor is cooled, filter, wash with distilled water and absolute ethanol in turn, and then dry in an oven at 80℃ for 10h; then place it in a muffle furnace at 450℃ for calcination for 4 hours, and finally in a tube furnace Calcined at 750°C for 3 hours to obtain iron-doped titanium nitride nanotubes.
[0040] Figure 5It is the SEM image of the iron-doped titanium nitride nanotube obtained in Example 3. The obtained iron-doped titanium nitride nanotube has an average diameter of 50-200nm, and is composed of iron-doped titanium nitride nanoparticle. It has a large specific surface ar...
PUM
| Property | Measurement | Unit |
|---|---|---|
| Diameter | aaaaa | aaaaa |
| The average diameter | aaaaa | aaaaa |
Abstract
Description
Claims
Application Information
Login to View More 
PatSnap Eureka turns technology decisions into work you can execute. Powered by our Innovation Knowledge Graph, it runs expert workflows across engineering, life sciences, materials and intellectual property. Get your review-ready output in minutes.
