Co-Ni co-doping anti-corrosion glass and preparation and use methods thereof
A corrosion-resistant glass, co-ni technology, applied in the field of corrosion-resistant glass, can solve the problems of coating corrosion, loss of steel protection effect, etc., to achieve the effect of preventing corrosion, low price and stable process
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Embodiment 1
[0029] Embodiment 1: Preparation and sealing of materials
[0030] According to the proportioning of each component of embodiment 1 in table 1, take a certain amount of analytically pure raw material (B 2 o 3 , SiO 2 、Na 2 O, K 2 O. Co 2 o 3 and Ni 2 o 3 ), use a planetary ball mill for 24 hours to mix evenly; then put the powder into a platinum crucible, place it in the air atmosphere of a box-type resistance furnace, heat it to 1100°C at 3°C / min, and keep it warm for 1 hour; then, take out the crucible, Pour the melt into deionized water for rapid cooling, and dry to obtain fragments of glass melt; grind and pass through a 100-mesh sieve to obtain glass powder. Mix glass powder with polyvinyl alcohol, fish oil, ethanol and toluene (80%, 2%, 1%, 10%, 7% by weight) to form a slurry, and disperse evenly in a ball mill; tape casting, natural Dry, then cut into the embryo body of the desired shape; place the embryo body on the part to be sealed, heat up in an electric fu...
Embodiment 2
[0031] Embodiment 2: Preparation and sealing of materials
[0032] According to the proportioning of each component of embodiment 2 in table 1, take a certain amount of analytically pure raw material (B 2 o 3 , SiO 2 、Na 2 O, K 2 O. Co 2 o3 and Ni 2 o 3 ), use a planetary ball mill for 24 hours to mix evenly; then put the powder into a platinum crucible, place it in the air atmosphere of a box-type resistance furnace, heat it at 3°C / min to 1020°C, and keep it warm for 1 hour; then, take out the crucible, Pour the melt into deionized water for rapid cooling, and dry to obtain fragments of glass melt; grind and pass through a 100-mesh sieve to obtain glass powder. Mix glass powder with methylcellulose, polyvinyl alcohol, n-butanol and acetone (82%, 2%, 2%, 8%, 6% by weight) to form a slurry, and disperse evenly in a ball mill; Stretching, drying naturally, and then cutting the embryo body into the desired shape; placing the embryo body on the part to be sealed, heating i...
Embodiment 3
[0033] Embodiment 3: Preparation and sealing of materials
[0034] According to the proportioning of each component of embodiment 3 in table 1, take a certain amount of analytically pure raw material (B 2 o 3 , SiO 2 、Na 2 O, K 2 O. Co 2 o 3 and Ni 2 o 3 ), use a planetary ball mill for 24 hours to mix evenly; then put the powder into a platinum crucible, place it in the air atmosphere of a box-type resistance furnace, heat it to 960°C at 3°C / min, and keep it warm for 1 hour; then, take out the crucible, Pour the melt into deionized water for rapid cooling, and dry to obtain fragments of glass melt; grind and pass through a 100-mesh sieve to obtain glass powder. Mix glass powder with epoxy resin, polyacrylamide, isopropanol and toluene (84%, 1.5%, 0.5%, 9%, 5% by weight) to form a slurry, and disperse evenly in a ball mill; casting Shaping, drying naturally, and then cutting into the embryo body of the desired shape; place the embryo body on the part to be sealed, hea...
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