Ceramic membrane prepared by using 3d (three-dimensional) printing technology and preparation method thereof
A 3D printing and ceramic membrane technology, applied in the direction of additive processing, etc., can solve the problems of difficult absorption and treatment of VOCs, secondary pollution, high processing cost, etc., and achieve the effect of good shock resistance, low preparation cost and simple process
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[0038] The preparation method of the ceramic membrane prepared by the 3D printing technology comprises the following steps:
[0039] S1: Soak vermiculite, quartz, calcium silicate, activated carbon, zeolite, and attapulgite in deionized water to wash off the attached pollutants, then dry them until the water content is ≤2%, and then dry the dried vermiculite , quartz, calcium silicate, activated carbon, zeolite, attapulgite, carbon fiber, and glass fiber are put into a nano pulverizer, pulverized at a speed of 1000-1200r / min for 1-1.5h, and passed through a sieve to obtain a mixture A;
[0040] S2: The mixture A prepared in step S1, tetrabutyl titanate, methyl isobutyl ketone, graphene, initiator, catalyst, and toughening agent are mixed at a temperature of 220-260°C and a speed of 400-600r / min After stirring for 2-3 hours, put it into a nano pulverizer to pulverize to obtain the mixture B;
[0041] S3: Mix the mixture B prepared in step S2, the tackifier, the coagulant, and ...
Embodiment 1
[0045] A ceramic membrane prepared by 3D printing technology, including the following raw materials in parts by weight: 105 parts of vermiculite, 65 parts of quartz, 30 parts of calcium silicate, 28 parts of activated carbon, 18 parts of zeolite, 16 parts of attapulgite, 17 parts of carbon fiber, 6 parts of tetrabutyl titanate, 8 parts of methyl isobutyl ketone, 4 parts of glass fiber, 1.6 parts of graphene, 0.4 parts of initiator, 0.7 parts of catalyst, 0.6 parts of tackifier, 1.6 parts of toughening agent 1 part, 1 part of coagulant, 0.7 part of stabilizer.
[0046] The initiator is azobisisobutyrate (ethylene glycol acrylate).
[0047] The catalyst is a platinum catalyst.
[0048] The tackifier is propyltrimethoxysilane.
[0049] The toughening agent is polypropylene rubber.
[0050] The coagulant is polyaluminum chloride.
[0051] The stabilizer is an organotin stabilizer.
[0052] The preparation method of the ceramic membrane prepared by the 3D printing technology c...
Embodiment 2
[0058] A ceramic membrane prepared by 3D printing technology, including the following raw materials in parts by weight: 90 parts of vermiculite, 55 parts of quartz, 24 parts of calcium silicate, 25 parts of activated carbon, 16 parts of zeolite, 14 parts of attapulgite, 13 parts of carbon fiber, 5 parts of tetrabutyl titanate, 6 parts of methyl isobutyl ketone, 3 parts of glass fiber, 1 part of graphene, 0.3 part of initiator, 0.5 part of catalyst, 0.4 part of tackifier, 1.2 parts of toughening agent part, 0.8 part of coagulant, and 0.5 part of stabilizer.
[0059] The initiator is azobisisobutyrate (ethylene glycol acrylate).
[0060] The catalyst is a platinum catalyst.
[0061] The tackifier is propyltrimethoxysilane.
[0062] The toughening agent is polypropylene adiene rubber.
[0063] The coagulant is polyaluminum chloride.
[0064] The stabilizer is an organotin stabilizer.
[0065] The preparation method of the ceramic membrane prepared by the 3D printing technolo...
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