Organoantimony crosslinking agent and its preparation method and cleaning fracturing fluid
A technology of cross-linking agent and organic antimony, which is applied in the field of organic antimony cross-linking agent and its preparation, and clean fracturing fluid, which can solve problems such as difficult to solve the performance requirements of construction-scale fracturing fluid, restrictions on wide application, and impact on fracturing effects , to achieve the effect of controlling the crack height, uniform sanding, and no protrusion in the rheological curve
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[0055] Another embodiment of the present invention proposes a preparation method of an organic antimony crosslinking agent, which includes the following steps:
[0056] 1) Synthesis of polyol antimonate: add sorbitol in isopropanol solvent, add antimony trichloride dropwise with stirring at 20°C-30°C, pass through ammonia gas to react for 90-120min, after the reaction, filter and distill , refined to obtain polyol antimonate;
[0057] 2) Add the polyol antimonate to triethanolamine under stirring state, react at 120-150° C. for 60-90 minutes, distill and refine after the reaction to obtain an organic antimony cross-linking agent.
[0058] The weight ratio of isopropanol, sorbitol, antimony trichloride and triethanolamine in the preparation method of the organic antimony crosslinking agent in the embodiment of the present invention is 50-70:10-30:5-10:10-30.
[0059] The dropping time of antimony trichloride in the preparation method of the organic antimony crosslinking agent ...
Embodiment 1
[0073] 1) Synthesis of polyol antimonate: Add 68g of sorbitol into 240g of isopropanol solvent, add 32g of antimony trichloride dropwise with stirring at 30°C, the antimony trichloride is added dropwise within 20min, and then pass through ammonia gas, React at 30°C for 120 minutes. After the reaction, remove ammonium chloride by filtration, and the filtrate is distilled and refined to obtain triethanolamine polyol antimonate crosslinking agent, which is polyol antimonate;
[0074] 2) Add the above-mentioned polyol antimonate to 60 g of triethanolamine under stirring, and react at 140° C. for 90 min. After the reaction, distill and refine to obtain an organic antimony crosslinking agent.
Embodiment 2
[0076] 1) Synthesis of polyol antimonate: Add 14g of sorbitol to 122g of isopropanol solvent, add 16g of antimony trichloride dropwise with stirring at 25°C, the antimony trichloride is added dropwise within 20min, and ammonia gas is passed in, React at 30°C for 90 minutes. After the reaction, remove ammonium chloride by filtration, and the filtrate is distilled and refined to obtain triethanolamine polyol antimonate crosslinking agent, which is polyol antimonate;
[0077] 2) Add the polyol antimonate to 48 g of triethanolamine under stirring, react at 120° C. for 70 min, distill and refine after the reaction to obtain an organic antimony crosslinking agent.
[0078] The organic antimony crosslinking agent in the clean fracturing fluid components of Examples 3-6 is the organic antimony crosslinking agent prepared in Example 1. Table 1 shows the components of the clean fracturing fluids of Examples 3-6.
[0079] The composition (percentage by weight) of the clean fracturing fl...
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