Method for preparing aqueous coating with automatic cleaning function
A water-based coating and self-cleaning technology, applied in the direction of coating, etc., can solve the problems of high construction environment requirements, environmental and human hazards, poor self-cleaning effect, etc., so as not to be easily polluted, reduce pollution, and have strong adhesion Effect
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Embodiment 1
[0012] Mix ammonium fluoride with a concentration of 1wt% and ethylene glycol according to a volume ratio of 1:5 to prepare an electrolyte; a volume concentration of 25vt% orthosilicate ethanol solution and a volume concentration of 15vt% hydrochloric acid solution according to a volume ratio of 1: 1.5 Mix evenly to prepare a modified solution; take high-purity titanium flakes and carry out anodic oxidation in the electrolyte, the oxidation voltage is 65V, oxidize for 10 hours, rinse the titanium flakes with a large amount of deionized water, and put titanium dioxide nanotubes in the modified Soak in the liquid for 2-3 hours, and dry naturally to obtain modified titanium dioxide nanotubes.
Embodiment 2
[0014] The water-based paint is made of the following raw materials by weight: 50g water, 15g polyvinyl alcohol, 20g acrylic resin, 5g dioctyl phthalate, 15g modified titanium dioxide nanotubes, 1g silicone defoamer, 12g triethanolamine, 0.5 g silane coupling agent KH570, 0.1 g sodium lauryl sulfate.
[0015] The preparation method of the water-based paint with automatic cleaning function is: first heat and melt the acrylic resin, slowly add polyvinyl alcohol, and stir for 30 minutes. min, after stirring for 0.5 hours, add silicone defoamer, stir for 0.5 hours, cool down to 50°C, add sodium lauryl sulfate and dioctyl phthalate, continue stirring for 1 hour, stop stirring, Add modified titanium dioxide nanotubes into the reaction kettle, after ultrasonic vibration for 1.5 hours, raise the temperature of the reaction kettle to 75°C for 2 hours, then add triethanolamine and silane coupling agent KH570, keep the temperature for 5 hours, close the reaction kettle to obtain the wate...
Embodiment 3
[0017] The water-based paint is made from the following raw materials by weight: 55g water, 20g polyvinyl alcohol, 21g acrylic resin, 6g dioctyl phthalate, 13g modified titanium dioxide nanotubes, 1.5g silicone defoamer, 11g triethanolamine, 0.3g silane coupling agent KH570, 0.4g sodium lauryl sulfate.
[0018] The preparation method of the water-based paint with automatic cleaning function is as follows: first heat and melt the acrylic resin, slowly add polyvinyl alcohol, stir for 25 minutes, after mixing evenly, add water into the stirring tank and heat to 90°C, the stirring speed is 500r / min, after stirring for 1 hour, add silicone defoamer, stir for 0.5 hours, cool down to 45°C, add sodium lauryl sulfate and dioctyl phthalate, continue stirring for 1 hour, stop stirring, Add modified titanium dioxide nanotubes into the reaction kettle, and after ultrasonic vibration for 1 hour, raise the temperature of the reaction kettle to 75°C for 2 hours, then add triethanolamine and ...
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