Method for producing wax for warm mix of asphalt from products synthesized by F-T
A synthetic product, F-T technology, applied in petroleum wax refining, petroleum industry, climate change adaptation and other directions, can solve the problems of reducing the mixing temperature of asphalt mixture, reducing the viscosity of asphalt at 60°C, and low production cycle of product yield, etc. The effect of low investment in equipment, low operating cost and simple production process
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Embodiment 1
[0051] This embodiment includes: (1) hydroconversion and (2) sweating.
[0052] (1) Hydroconversion
[0053]The wax oil product (normal paraffin content: 95.5wt%; drop melting point: 86.2°C; needle penetration (25°C) 55 (10 -1 mm)) as raw material, in the FHJ-2 catalyst (a Ni / Al 2 o 3 Commercial catalyst, developed and produced by Fushun Petrochemical Research Institute, the content of active metal nickel in terms of oxides is 40%, and the catalyst is subjected to conventional reduction treatment before use), under the action of reaction pressure 5.0MPa, reaction temperature 200°C, volume space velocity 1.0 h -1 Hydrogenation is carried out at a volume ratio of 500:1 to hydrogen to convert olefins and oxygenates therein.
[0054] Hydrogenation product properties: n-paraffin weight content 97.36%; drop melting point 85.0°C; needle penetration (25°C) 57 (10 -1 mm); Chromatography-mass spectrometry analysis, no alcohol, alkene, acid and other substances were detected.
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Embodiment 2
[0073] This embodiment includes: (1) hydroconversion and (2) sweating.
[0074] (1) Hydroconversion
[0075] With embodiment 1.
[0076] (2) sweating
[0077] This part includes: (1) preparation work, (2) cooling down - constant temperature crystallization, (3) heating up - constant temperature sweating, (4) product refining and other processes.
[0078] (1) Preparation
[0079] Connect the jacket of the sweating dish and the movable coil to the circulation system, and fix the coil on the sweating dish; use the heat transfer oil as the medium; start the heating function of the circulation system to raise the temperature of the heat transfer oil to 90°C. Put water under the sweating dish plate.
[0080] Install the sealing system on the upper part of the sweating dish and connect it to the pressurized buffer tank and the compressor; install the decompression buffer tank on the lower part of the sweating dish and connect it to the vacuum pump; connect the pressurized buffer ...
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