Synthetic method of resveratrol intermediate p-hydroxy benzaldehyde
A technology of p-hydroxybenzaldehyde and resveratrol, which is applied in the field of medicine, can solve the problems of catalyst recovery and mechanical application, and achieve the effects of low pollution, simple post-treatment, and mild reaction conditions
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Image
Examples
Embodiment 1-1
[0021] Put 4g of porous silicon KIT-6 and 30mL of xylene into a reaction vessel, stir in an oil bath at 70°C for 1 hour to obtain a mixed solution of KIT-6 and xylene; dissolve 1g of copper nitrate and 1g of cobalt nitrate in 4mL of water, A metal nitrate solution was obtained; then the metal nitrate solution was added dropwise to the mixed solution of KIT-6 and xylene, and continued to stir at 70°C for 8h. Filter, wash with water, dry at 100°C for 8 hours, and bake at 490°C for 4 hours to obtain a copper-cobalt composite metal oxide catalyst. figure 1 It is an electron microscope picture of copper-cobalt composite metal oxide, which has a large surface area and pore volume, and adjustable pore diameter (2-50nm).
Embodiment 1-2
[0023] Put 4g of porous silicon KIT-6 and 30mL of xylene into a reaction vessel, stir in an oil bath at 70°C for 1 hour to obtain a mixed solution of KIT-6 and xylene; dissolve 2g of nickel nitrate and 2g of cobalt nitrate in 4mL of water, A metal nitrate solution was obtained; then the metal nitrate solution was added dropwise to the mixed solution of KIT-6 and xylene, and continued to stir at 70°C for 8h. Filtrate, wash with water, dry at 120°C for 4 hours, and bake at 510°C for 2 hours to obtain a nickel-cobalt composite metal oxide catalyst. It can be seen from the electron micrograph that the catalyst has a larger surface area and pore volume, and an adjustable pore diameter (2-50nm).
Embodiment 1-3
[0025] Put 4g of porous silicon KIT-6 and 30mL of xylene into a reaction vessel, stir in an oil bath at 70°C for 1 hour to obtain a mixed solution of KIT-6 and xylene; dissolve 3g of manganese nitrate and 3g of cobalt nitrate in 4mL of water, A metal nitrate solution was obtained; then the metal nitrate solution was added dropwise to the mixed solution of KIT-6 and xylene, and continued to stir at 70°C for 8h. Filter, wash with water, dry at 110°C for 6 hours, and bake at 500°C for 3 hours to obtain a manganese-cobalt composite metal oxide catalyst. It can be seen from the electron micrograph that the catalyst has a larger surface area and pore volume, and an adjustable pore diameter (2-50nm).
PUM
Login to View More Abstract
Description
Claims
Application Information
Login to View More