Organic crystalline state material on the basis of rare earth metal europium, preparation, and application thereof in fluorescent recognition of antibiotics
A technology of rare earth metals and metal organic frameworks, applied in the fields of luminescent materials, fluorescence/phosphorescence, material excitation analysis, etc., can solve rare problems, achieve low temperature requirements, high yield, and easy control
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[0040] (1) Take 0.5mmol of triazine polycarboxylic acid, 1mmol of europium nitrate, 5ml of DMF, 0.5ml of H 2 O, 0.025ml with a concentration of 0.1mol / L NaOH, 0.3ml of 3.5M nitric acid, add it to a stainless steel reactor lined with polytetrafluoroethylene, react at a constant temperature at 160°C for 72h, and cool down at a constant rate of 2-3°C / h to At room temperature, a colorless transparent block crystal is obtained, namely 4,4',4"-s-triazine-1,3,5-tris-m-aminobenzoic acid rare earth Eu metal organic framework crystalline material.
[0041] (2) Add 5mg of 4,4',4"-s-triazine-1,3,5-tris-m-aminobenzoic acid rare earth Eu metal organic framework crystal material to 10ml containing the selected antibiotic concentration In a 0.1mmol / L aqueous solution system (the antibiotics are FCC, FDZ, PCL, FZD, NFT, CAP, NZF, SMZ, RDZ, MDZ, DTZ, ODZ), ultrasonic vibration at room temperature for 0.5h, take out and load In a 4ml four-sided transparent cuvette, the fluorescence intensity was te...
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