The invention relates to a rare earth terbium-based metal organic framework material, a synthesis method and its application in antibiotic identification. The chemical molecular formula of the metal organic framework material is {[Tb(TATAB)(H 2 O)]·2H 2 O} n , TATAB is an organic ligand 4,4′,4″-s-triazine-1,3,5-three-m-aminobenzoic acid. The basic structural unit contains a free terbium ion and a complete 4,4 ′,4″‑s‑triazine‑1,3,5‑tri‑m-aminobenzoic acid, the three carboxyl groups in the ligand are deprotonated to bridge adjacent terbium ions, and each terbium ion is bound to five ligands It is coordinated with a water molecule, and two carboxyl groups are respectively connected with two different terbium ions to form a three-dimensional network structure. The material is simple to prepare, has a novel structure, is stable in aqueous solution, and can rapidly detect metronidazole (MDZ), ornidazole (ODZ), ronidazole (RDZ), and dimetazole (DTZ) in aqueous solution.