Hydrocracking catalyst intermediate, hydrocracking catalyst, and preparation methods of hydrocracking catalyst intermediate and hydrocracking catalyst
A hydrocracking and catalyst technology, applied in the field of hydrocracking catalysts and their preparation, and hydrocracking catalyst intermediates, can solve problems such as excessive temperature rise, and achieve sufficient sulfidation, good metal dispersion, and good hydrogenation performance Effect
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Embodiment 1
[0060] Example 1 Preparation of Hydrocracking Catalyst A
[0061] Weigh 26.5 g of ammonium molybdate, 25 g of nickel nitrate, and 50 mL of ammonia water, and mix them with deionized water to 100 mL to obtain solution I. Dissolve 30 g of 2,4,6-trimercapto-s-triazine triammonium salt in 50 mL of water to obtain solution II. Weigh 12.7 grams of Y molecular sieve (SiO 2 / Al 2 o 3 The molar ratio is 16, and the specific surface area is 613m 2 / g, total pore volume 0.48mL / g), 35.5 grams of amorphous silicon aluminum (SiO 2 Content 50wt%, pore volume 0.85ml / g, specific surface area 370m 2 / g, dry basis 70wt%) and 61.5 grams of macroporous alumina (pore volume 1.0ml / g, specific surface area 400m 2 / g, dry basis 70wt%), then put into 2L water, after vigorously stirring for 20min, add solutions I and II side by side, then stir for another 30min, wash, and filter with suction. The filter cake obtained by suction filtration was heat-treated at a low temperature of 80° C. for 3 hour...
Embodiment 2
[0062] Example 2 Preparation of Hydrocracking Catalyst B
[0063] Take 21.8g of molybdenum oxide, 10.7g of basic nickel carbonate, 2mL of phosphoric acid, and 60mL of deionized water, mix them uniformly and boil for 1 hour to obtain solution I. Weigh 42 g of 2,4-dimercapto-s-triazine diammonium salt and dissolve it in 100 mL of acetone solution to obtain solution II. Weigh 12.7 grams of Y sieve (SiO 2 / Al 2 o 3 The molar ratio is 16, and the specific surface area is 613m 2 / g, total pore volume 0.48mL / g), 35.5 grams of amorphous silicon aluminum (SiO 2 Content 50wt%, pore volume 0.85ml / g, specific surface area 370m 2 / g, dry basis 70wt%) and 61.5 grams of macroporous alumina (pore volume 1.0ml / g, specific surface area 400m 2 / g, dry basis 70wt%), then put it into 2L of water, after vigorously stirring for 20min, drop solution I into the slurry and stir for 10min, then drop solution II into the slurry, stir vigorously during the dropping process, and then stir for 30min A...
Embodiment 3
[0064] Example 3 Preparation of Hydrocracking Catalyst C
[0065] Prepare the solution I of Example 1 with the same mass and concentration. Dissolve 75 g of 2,4,6-trimercapto-s-triazine monoammonium salt in 50 mL of water to obtain solution II. Weigh 9.7 grams of Y molecular sieve (SiO 2 / Al 2 o 3 The molar ratio is 16, and the specific surface area is 613m 2 / g, total pore volume 0.48mL / g), 12.2 grams of β molecular sieve (SiO 2 / Al 2 o 3 The molar ratio is 82, and the specific surface area is 546m 2 / g, total pore volume 0.46mL / g) and 100 grams of macroporous alumina (pore volume 1.0ml / g, specific surface area 400m 2 / g, dry basis 70wt%), then put into 2L water, after vigorously stirring for 20min, add solutions I and II side by side, then stir for another 30min, wash, and filter with suction. Other steps were the same as in Example 1 to obtain hydrocracking catalyst C, whose main physical properties are shown in Table 1.
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