Environmentally friendly water-based mold release composition
An environment-friendly, composite technology, applied in the direction of lubricating compositions, petroleum industry, etc., can solve the problems of no good economic benefits, no energy saving and environmental protection, high labor costs, etc., achieve superior anti-sticking mold function, improve production progress, The effect of reducing labor costs
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[0057] The second aspect of the present invention provides a kind of preparation method of environment-friendly water-based mold release composition as above, comprises the steps:
[0058] Add oxidized polyethylene wax, sodium dioctyl succinate, polyacrylamide, and deionized water into the container, add alkyl silicone oil under stirring, stir at 200-300rpm, stir for 10-20min, and heat to 35°C, then add sulfonated methylcellulose, cyclodextrin, imidazoline compounds, and isothiazolinone compounds, keep warm for 10 minutes, then heat to 50°C, adjust the stirring speed to 500-600rpm, and add fatty alcohol in turn Polyoxyethylene ether, solvent naphtha, and polyvinyl alcohol were continuously stirred at 50°C for 10 minutes, then cooled to room temperature, then added with isopropanol and isopropanolamine, and stirred evenly to obtain the product.
[0059] The preparation method of the invention can prevent the composition from agglomerating in water, facilitate the dissolution of...
Embodiment
[0062] A1 3-Hexylheptamethyltrisiloxane
[0063] A2 Heptamethyltrisiloxane
[0064] A3 dimethicone
[0065] B1 polyvinyl alcohol PVA2488
[0066] B2 polyvinyl alcohol PVA2499
[0067] C sulfonated methyl cellulose
[0068]The preparation method of sulfonated methylcellulose is: stir 8.4g methylcellulose in 50mL 30wt% hydrogen peroxide aqueous solution for 1h, then evaporate the solvent to dryness with a rotary evaporator, add 50mL tetrahydrofuran, and then cool in an ice bath , keep the temperature below 5°C, add 1.2mL of chlorosulfonic acid dropwise, and then continue to stir for 2h. After the reaction, evaporate the solvent to dryness with a rotary evaporator, wash with acetone three times, use 10mL each time, and then vacuum dry for 5h. have to.
[0069] Dβ-cyclodextrin
[0070] E D40 solvent oil
[0071] F Isopropanol
[0072] G oxidized polyethylene wax
[0073] Sodium diisooctylsulfonate H succinate
[0074] IPolyacrylamide
[0075] J Isopropanolamine
[0076...
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