Composite membrane for latent fingerprint transfer or developing or content integrated full-dry state detection and detection method
A detection method and a composite membrane technology, applied in the detection field, can solve problems such as insensitivity, cumbersome operation, light color development, etc., and achieve the effects of favorable preservation, realization of transfer, and low adsorption force
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Embodiment 1
[0043] Example 1, Preparation of AgNPs@PDA@PDMS Composite Membrane
[0044] The preparation method of AgNPs@PDA@PDMS composite membrane, the synthetic route is as follows figure 1 As shown in a:
[0045] Wherein, method one step is as follows:
[0046] (1) Synthesis of polydimethylsiloxane (PDMS) membrane: Weigh 3g of PDMS prepolymer and 0.3g of hardener (Sylgard 184, Dow Corning) in a plastic petri dish with a diameter of 9cm, mix well, and then vacuumize Make the air bubbles in the mixture float to the surface and burst, and then place it on a heating platform at 60-100°C for 2-4 hours to obtain PDMS films with different hardness;
[0047] (2) Synthesis of polydopamine@polydimethylsiloxane (PDA@PDMS) membrane: take 15ml Tris-HCl (50mM, pH=8.5) buffer solution, put it in a clean beaker, add 30mg dopamine hydrochloride, 30mg over Ammonium sulfate, stirred for 1min, poured into a petri dish with PDMS membrane, reacted at room temperature (18-25°C) for 5min-2h, rinsed with wate...
Embodiment 2
[0053] Example 2. Development and imaging of latent fingerprints using AgNPs@PDA@PDMS composite film
[0054] Using AgNPs@PDA@PDMS composite film latent fingerprint development and imaging process as follows figure 1 As shown in b, the specific steps are as follows:
[0055] A. Latent fingerprint treatment: drop 5 μl of different concentrations of rhodamine 6G (Rhodamine6g, R6g), p-aminothiophenol (4-Aminothiophenol, 4-ATP), methyl blue (methyl blue) or For thiabendazole solution, let it stand for 10 minutes to volatilize the solution, press fingerprints on the carrier material, leave it in the air for 1-3 days, or heat it at 60°C for 15-60 minutes, or blow it with an electric hair dryer for 5 minutes.
[0056] B. Gently attach the AgNPs@PDA@PDMS composite film to the fingerprint carrier material, and separate after standing for 5 minutes, and obtain the latent fingerprint patterns visible to the naked eye on the original substrate and PDMS respectively;
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