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Biomass acid material and preparation method thereof

A biomass material and biomass technology, which is applied in the field of natural products and circular economy, can solve the problems of difficult recycling, heavy air pollution, and non-green environmental protection.

Active Publication Date: 2017-12-01
南京汉旗新材料股份有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0008] At present, the introduction of biomass acidic groups mainly adopts esterification method. The esterification reagents are mainly oleum, chlorosulfonic acid, sulfur trioxide, etc., and the solvents used are mainly dimethyl sulfoxide, N,N-dimethylmethane, etc. Amides, pyridine, etc., heavy air pollution, highly toxic solvents and difficult to recycle, do not meet the requirements of green environmental protection

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0023] In the flask, put coconut shell powder, glyoxylic acid and ethanol, the mass ratio is 1:0.5:10, the reaction temperature is 60°C, the reaction time is 2 hours, and the acidic coconut shell powder material is obtained by filtration, with a yield of 92%. Surface acidity is 3.5.

Embodiment 2

[0025] In the flask, put wood flour, propionic acid and ethanol, the mass ratio is 1:2:20, the reaction temperature is 78°C, the reaction time is 10 hours, and the acidic wood flour material is obtained by filtration, the yield is 98%, and the surface acidity is 3.6.

Embodiment 3

[0027] In the flask, put bamboo powder, uronic acid and ethanol, the mass ratio is 1:0.2:3, the reaction temperature is 30°C, the reaction time is 2 hours, and the acidic coconut shell powder material is obtained by filtration, the yield is 81%, the surface The acidity is 4.1.

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PUM

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Abstract

The invention discloses a biomass acid material which is obtained through reaction of a biomass material and aldehyde acid, wherein the biomass material contains one or more of active groups, namely hydroxyl, amino, an aldehyde group or an ester group. According to the biomass acid material, leftover materials of natural plant resources are utilized, so that additional resource consumption is not needed and the biomass acid material meets the circular economy requirement.

Description

technical field [0001] The invention belongs to the field of natural products and circular economy, and in particular relates to the modification and preparation of a biomass acid material. Background technique [0002] Biomass materials use woody plants, grasses and vines and their processing residues and wastes as raw materials, and process and manufacture new materials with excellent performance and high added value through high-tech means such as physics, chemistry and biology. [0003] Coir (Latin name: Cocos Nucifera L. ) is the endocarp of the palm plant coconut. After drying, the horny flakes are brownish brown and extremely hard. Chemical Composition Coconut shell contains 0.61% ash, 36.51% lignin, 53.06% cellulose, and 29.27% ​​(total amount) of pentosan. [0004] The powder made of wood is called wood powder, which generally refers to the leftover scraps from wood processing in furniture factories, MDF factories, and multilayer board factories. The main compone...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C08H8/00
CPCC08H8/00
Inventor 孟庆华朱虹李忠李建红程道远
Owner 南京汉旗新材料股份有限公司
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