Fertilizer special for grapes and preparation method of fertilizer
A special fertilizer and grape technology, applied in the field of fertilizer production, to achieve the effects of small dosage, improved synergy, and increased nutrient content
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Embodiment 1
[0040] A. Raw material pretreatment
[0041] (1) Take sugarcane tips and leaves, remove impurities, crush them with a pulverizer to obtain raw material slag, and then send them to a steam blaster for blasting treatment to obtain bagasse powder;
[0042] The steam explosion treatment is carried out in two stages. The steam explosion pressure of the first stage is 1.6MPa, and the pressure holding time is 200s; the steam explosion steam pressure of the second stage is 2.8MPa, and the pressure holding time is 140s.
[0043] (2) Add bagasse powder to 5-8% of its mass in ionic liquid, heat and stir to 80°C under nitrogen protection, keep warm for 10 minutes, then add 10% solid acid catalyst, heat to 200°C, and react for 5 hours to obtain a degradation mixture;
[0044] Described ionic liquid is made up of cholyl cation and glycine anion, and its water content is 80%;
[0045] (3) Cool down the degradation mixture to 60°C, add an equal volume of warm water at 60°C, mix well, centri...
Embodiment 2
[0053] A. Raw material pretreatment
[0054] (1) Take sugarcane tips and leaves, remove impurities, crush them with a pulverizer to obtain raw material slag, and then send them to a steam blaster for blasting treatment to obtain bagasse powder;
[0055] The steam explosion treatment is divided into two stages, the first stage explosion steam pressure is 1.2MPa, and the pressure holding time is 240s; the second stage steam explosion steam pressure is 2MPa, and the pressure holding time is 160s.
[0056] (2) Add bagasse powder to 5% ionic liquid by mass, heat and stir to 60°C under nitrogen protection, keep warm for 10min, then add 5% solid acid catalyst, heat to 180°C, and degrade after 3h of reaction time mixture;
[0057] Described ionic liquid is made up of cholyl cation and alanine anion, and its water content is 50%;
[0058] (3) Cool down the degradation mixture to 50°C, add an equal volume of warm water at 50°C, mix well, centrifuge at 17000rpm for 15min, wash the resi...
Embodiment 3
[0066] A. Raw material pretreatment
[0067] (1) Take sugarcane tips and leaves, remove impurities, crush them with a pulverizer to obtain raw material slag, and then send them to a steam blaster for blasting treatment to obtain bagasse powder;
[0068] The steam explosion treatment is divided into two stages, the first stage explosion steam pressure is 1.4MPa, and the pressure holding time is 220s; the second stage steam explosion steam pressure is 2.2MPa, and the pressure holding time is 150s.
[0069] (2) Add bagasse powder to 6% of its mass ionic liquid, heat and stir to 65°C under nitrogen protection, keep warm for 10min, then add 6% solid acid catalyst, heat to 180°C, and degrade after 4h of reaction time mixture;
[0070] Described ionic liquid is made up of cholyl cation and lysine anion, and its water content is 60%;
[0071] (3) Cool down the degradation mixture to 50°C, add an equal volume of warm water at 50°C, mix well, centrifuge at 17,000rpm for 20min, wash th...
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