Complex of twice-complexed zinc, as well as preparation method and usage thereof
A technology of complexes and zinc complexes, which is applied in the field of complexes, can solve the problems of high cost of use, and achieve the effects of avoiding waste, reducing cost of use, and good solubility
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Embodiment 1
[0047] A secondary zinc complex made from sucrose, zinc sulfate and amino acids.
[0048] The preparation method of the complex of described secondary complex zinc comprises the following steps:
[0049] (1) Add 25 parts by weight of sucrose in the reactor, add 50 parts by weight of water to dissolve the sucrose, add 30 parts by weight of zinc sulfate, alkalinize the aqueous solution of sodium hydroxide, adjust the pH of the solution to 11, heat the reactor, Keep the temperature in the kettle between 70-80°C, carry out the complexation reaction for 1 hour, continuously stir during the reaction process, generate a sucrose zinc solution, filter and separate, obtain the filter residue A and filtrate a, add 75% of 2 times the weight of the filtrate a The ethanol solution is precipitated, and after the precipitation is complete, it is centrifugally filtered to obtain the filter residue B and the filtrate b. The filter residue B is vacuum-dried and dried, sieved and detected, and th...
Embodiment 2
[0053] A secondary zinc complex made from sucrose, zinc sulfate and amino acids.
[0054] The preparation method of the complex of described secondary complex zinc comprises the following steps:
[0055] (1) Add 32 parts by weight of sucrose in the reactor, add 60 parts by weight of water to dissolve the sucrose, add 35 parts by weight of zinc sulfate, alkalinize the aqueous solution of sodium hydroxide, adjust the pH of the solution to 12, heat the reactor, Keep the temperature in the kettle between 70-80°C, carry out the complexation reaction for 2 hours, continuously stir during the reaction process, generate sucrose zinc solution, filter and separate, obtain filter residue A and filtrate a, add 75% of 2 times the weight of filtrate a The ethanol solution is precipitated, and after the precipitation is complete, it is centrifugally filtered to obtain the filter residue B and the filtrate b. The filter residue B is vacuum-dried and dried, sieved and detected, and the sucrose...
Embodiment 3
[0059] A secondary zinc complex made from sucrose, zinc sulfate and amino acids.
[0060] The preparation method of the complex of described secondary complex zinc comprises the following steps:
[0061] (1) Add 28 parts by weight of sucrose in the reactor, add 55 parts by weight of water to dissolve the sucrose, add 32 parts by weight of zinc sulfate, alkalinize the aqueous solution of sodium hydroxide, adjust the pH of the solution to 12, heat the reactor, Keep the temperature in the kettle between 70-80°C, carry out the complexation reaction for 1.5h, stir continuously during the reaction process, generate sucrose zinc solution, filter and separate, obtain filter residue A and filtrate a, add 2 times the weight of 75 % ethanol solution for precipitation, after the precipitation is complete, centrifuge and suction filter to obtain filter residue B and filtrate b, filter residue B is vacuum-dried and dried, sieved and detected, and the sucrose zinc product is obtained; the fi...
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