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A kind of preparation method of microcapsule embedded globulin

A production method and globulin technology, applied in the field of protein deep processing, can solve the problems of inability to improve the health care property of wall materials, and achieve the effects of enhancing compactness, increasing health care property, and improving oxygen resistance

Inactive Publication Date: 2021-02-02
HENAN UNIVERSITY OF TECHNOLOGY
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The wall materials used in this patent are all made of pectin substances through enzymatic hydrolysis, which cannot improve the health care of the wall materials

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0021] A kind of preparation method of microcapsule embedded globulin, it is characterized in that: comprise the following steps:

[0022] (1) Solution preparation: 5 parts of magnetic bead powder, 1 part of ethyl cellulose, 1 part of Tween, 2 parts of gum arabic, 2 parts of gelatin, 2 parts of acetic acid, mix the above parts by weight evenly, and adjust the pH3 at 40 °C ;

[0023] (2) Homogenization: Use a high-speed homogenizer to emulsify and homogenize at 5000r / min for 10 minutes, and react for 1 hour;

[0024] (3) Settlement: After the mixture is cooled to room temperature, put it in the refrigerator, pour it into a mold to solidify and set it, and let it stand until the microcapsules settle;

[0025] (4) Core material: The globulin is freeze-dried at -70°C into powder, crushed and passed through a 300-mesh sieve.

[0026] (5) Embedding: Mix the wall material and the core material to make a solution with a content of 30%, add 1 part of vitamin C powder, and spray dry u...

Embodiment 2

[0028] A kind of preparation method of microcapsule embedded globulin, it is characterized in that: comprise the following steps:

[0029] (1) Solution preparation: 8 parts of magnetic bead powder, 3 parts of ethyl cellulose, 3 parts of Tween, 5 parts of gum arabic, 5 parts of gelatin, 5 parts of acetic acid, mix the above parts by weight evenly, and adjust the pH4 at 45 °C ;

[0030] (2) Homogenization: Use a high-speed homogenizer to emulsify and homogenize at 5500r / min for 15 minutes, and react for 2 hours;

[0031] (3) Settlement: After the mixture is cooled to room temperature, put it in the refrigerator, pour it into a mold to solidify and set it, and let it stand until the microcapsules settle;

[0032] (4) Core material: The globulin is freeze-dried at -60°C into powder, crushed and passed through a 500-mesh sieve.

[0033] (5) Embedding: Mix the wall material and the core material to make a 40% solution, add 3 parts of vitamin C powder, and spray dry at the inlet te...

Embodiment 3

[0035] A kind of preparation method of microcapsule embedded globulin, it is characterized in that: comprise the following steps:

[0036] (1) Solution preparation: 10 parts of magnetic bead powder, 5 parts of ethyl cellulose, 5 parts of Tween, 8 parts of gum arabic, 8 parts of gelatin, 7 parts of acetic acid, mix the above parts by weight evenly, and adjust the pH5 at 60 °C ;

[0037] (2) Homogenization: Use a high-speed homogenizer to emulsify and homogenize at 6000r / min for 30 minutes, and react for 3 hours;

[0038] (3) Settlement: After the mixture is cooled to room temperature, put it in the refrigerator, pour it into a mold to solidify and set it, and let it stand until the microcapsules settle;

[0039] (4) Core material: Freeze-dry globulin into powder at 0°C, crush it and pass it through a 1000-mesh sieve.

[0040] (5) Embedding: Mix the wall material and the core material to make a 50% solution, add 5 parts of vitamin C powder, and spray dry at an inlet temperatur...

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PUM

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Abstract

The invention relates to a method for making globulin embedded in microcapsules, which belongs to the technical field of protein deep processing; it includes a core material and a wall material, wherein the wall material is prepared from magnetic bead powder and ethyl cellulose; the invention adds magnetic beads The wall material compounded with powder and carbon fiber has the functions of whitening and promoting intestinal peristalsis, increasing the health care of the product, and at the same time enhancing the compactness, greatly improving the ability of oxygen resistance, heat resistance and light resistance.

Description

technical field [0001] The invention relates to the preparation of microcapsules, in particular to a method for preparing globulin embedded in microcapsules, and belongs to the technical field of protein deep processing. Background technique [0002] Globulin is a serum protein that exists in the human body. Globulin is a common protein that basically exists in all animals and plants. Globulin has an immune function, so it is also called immunoglobulin. When the immune system encounters a foreign invader, it will produce different amounts of globulin according to the different invaders. If the invader is difficult to eliminate, the immune system will stimulate the lymph and produce more globulin until the invader is eliminated by the globulin. . However, globulin is easily affected by the external environment, and factors such as heat, light, and oxygen will reduce its activity. Therefore, in order to maintain the activity of the protein and accurately perform the functio...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): B01J13/04B01J13/02A23L33/17A23P10/30
Inventor 吴丽黄继红纪小国侯银臣李海月赵祎张亚奇杨铭乾冯军伟
Owner HENAN UNIVERSITY OF TECHNOLOGY