Zirconium-oxide-based nanocomposite ceramic die material and preparation method thereof
A nano-composite, ceramic mold technology, applied in the field of ceramic mold materials, can solve the problem of low comprehensive mechanical properties of mold materials, and achieve the effects of good comprehensive mechanical properties, lower sintering temperature, and excellent anti-friction and wear resistance.
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[0018] Example 1
[0019] A zirconia-based nano composite ceramic mold material. The raw materials include 80 parts by weight of zirconia, 4 parts of silicon carbide, 8 parts of alumina, 1 part of lanthanum oxide, 2 parts of zinc oxide, 1 part of titanium oxide, and 0.8 parts of molybdenum. Parts, nickel 1 part, magnesium oxide 1 part.
[0020] Wherein, the particle size of the zirconia is 300-500nm; the particle size of the silicon carbide is 30-60nm; the particle size of the aluminum oxide, lanthanum oxide, and zinc oxide is 100-150nm.
[0021] The titanium oxide is doped with silicon oxide, and the specific modification method is as follows: prepare the titanium oxide into a 20g / L suspension, adjust the pH of the suspension to 10 with 0.5M sodium hydroxide solution, ultrasonically disperse, and increase the temperature. To 85°C, add 1mol / L sodium silicate aqueous solution dropwise to the suspension with stirring, the amount of sodium silicate is m(SiO 2 ): m(TiO 2 )=1:4, after dr...
Example Embodiment
[0030] Example 2
[0031] A zirconia-based nanocomposite ceramic mold material. The raw materials include 90 parts by weight of zirconia, 6 parts of silicon carbide, 11 parts of alumina, 2 parts of lanthanum oxide, 3 parts of zinc oxide, 2 parts of titanium oxide, and 1.2 parts of molybdenum. Parts, 1.1 parts of nickel and 2 parts of magnesium oxide.
[0032] Wherein, the particle size of the zirconia is 300-500nm; the particle size of the silicon carbide is 30-60nm; the particle size of the aluminum oxide, lanthanum oxide, and zinc oxide is 100-150nm.
[0033] The titanium oxide is doped with silicon oxide, and the specific modification method is as follows: prepare the titanium oxide into a 20g / L suspension, adjust the pH of the suspension to 10 with 0.5M sodium hydroxide solution, ultrasonically disperse, and increase the temperature. To 85°C, add 1mol / L sodium silicate aqueous solution dropwise to the suspension under stirring conditions. The amount of sodium silicate is m(SiO 2...
Example Embodiment
[0042] Example 3
[0043] A zirconia-based nanocomposite ceramic mold material. The raw materials include 100 parts by weight of zirconia, 10 parts of silicon carbide, 15 parts of alumina, 4 parts of lanthanum oxide, 5 parts of zinc oxide, 3 parts of titanium oxide, and 1.5 parts of molybdenum. Parts, 1.2 parts of nickel and 1.3 parts of magnesium oxide.
[0044] Wherein, the particle size of the zirconia is 300-500nm; the particle size of the silicon carbide is 30-60nm; the particle size of the aluminum oxide, lanthanum oxide, and zinc oxide is 100-150nm.
[0045] The titanium oxide is doped with silicon oxide, and the specific modification method is as follows: prepare the titanium oxide into a 20g / L suspension, adjust the pH of the suspension to 10 with 0.5M sodium hydroxide solution, ultrasonically disperse, and raise the temperature To 85°C, add 1mol / L sodium silicate aqueous solution dropwise to the suspension under stirring conditions. The amount of sodium silicate is m(SiO 2...
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