Three-sources-integrated intumescent flame retardant, and synthesis method and application thereof
A technology of intumescent flame retardant and synthesis method, which is applied in chemical instruments and methods, compounds of Group 5/15 elements of the periodic table, organic chemistry, etc. problems, to achieve the effect of high synthesis efficiency, mild reaction conditions and safe operation
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specific Embodiment approach 1
[0034] Specific implementation mode 1: The structural formula of the three-source intumescent flame retardant in this implementation mode is:
[0035]
[0036] where n≥1.
specific Embodiment approach 2
[0037] Specific embodiment two: The synthesis method of the three-source intumescent flame retardant in this embodiment includes the following steps:
[0038] 1. Add piperazine and distilled water to a four-neck flask equipped with a stirring device, a constant pressure dropping funnel, a thermometer and a reflux condenser. The mass ratio of piperazine and distilled water is 1:1, and heat until completely dissolved;
[0039] Add distilled water to the methylphosphonic acid to dissolve the methylphosphonic acid at room temperature to obtain a saturated aqueous solution of methylphosphonic acid, drop the saturated aqueous solution of methylphosphonic acid into a four-necked flask through a constant pressure dropping funnel, and add dropwise After completion, raise the temperature of the system to 85-90°C, react at this temperature for 3-5 hours, then place the colorless, transparent, viscous liquid obtained in a rotary evaporator for concentration, and then put it in a vacuum dry...
specific Embodiment approach 3
[0041] Embodiment 3: The difference between this embodiment and Embodiment 2 is that the molar ratio of methylphosphonic acid to piperazine in step 1 is 2:1. Others are the same as in the second embodiment.
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