Nano silver bamboo charcoal fiber and sterilization underwear product made of same
A nano-silver bamboo charcoal and fiber technology, applied in the field of clothing, can solve the problems of weakened sterilization effect of nano-silver, weak interaction between nano-silver and fabrics, etc.
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[0043] The preparation raw material of described nanovesicle at least comprises silver nitrate, bamboo charcoal nanopowder, and the preparation method of described nanovesicle is as follows:
[0044] (1) The polystyrene microsphere dispersion is added to the polyethyleneimine solution under stirring, after stirring for 30 minutes, after washing with deionized water, the modified polystyrene microspheres are obtained;
[0045] Wherein, the concentration of the polystyrene microsphere dispersion is 80mg / mL, and the number of parts is 2.5mL, the concentration of the polyethyleneimine solution is 0.6wt%, and the number of parts is 10mL, the modified polystyrene prepared above The microspheres were redispersed in 25 mL of water to obtain a modified polystyrene microsphere dispersion with a mass concentration of 8 mg / mL.
[0046] (2) Add 100 μL of 0.1M silver nitrate to 40 mL of deionized water, then weigh 40 mg of polyvinylpyrrolidone (PVP-K30) and add, stir and mix to obtain a mix...
Embodiment approach
[0053] As an embodiment of the present invention, the water-based polymer material is a composite of hydroxymethyl cellulose and chitosan cellulose, and the specific preparation method is as follows: add hydroxymethyl cellulose, chitosan Sugar cellulose, sodium lauryl sulfate, deionized water, raise the temperature to 60°C, keep warm for 10 minutes, and keep warm for 30 minutes at 30°C to obtain a water-based polymer material.
[0054] Modified chitosan:
[0055] The modified chitosan described in the present invention is quaternary ammonium salt modified chitosan.
[0056] The specific preparation method is as follows: (1) Add epichlorohydrin to the reactor, heat up to 75°C, slowly add long-chain alkyl tertiary amine dropwise, after the dropwise addition, stir for 0.5h, cool down to 55°C, add acetonitrile, and divide Add 1-hydroxyethyl-2-methyl-5-nitroimidazole for 3 times, keep the temperature for 8h, cool to room temperature, concentrate under reduced pressure to obtain th...
Embodiment 1
[0080] This embodiment provides a nano-silver bamboo charcoal fiber. The preparation raw materials of the nano-silver bamboo charcoal fiber at least include: nanovesicles, bamboo charcoal powder, water-based polymer material, modified chitosan, and additives.
[0081] The preparation method of described nanovesicle is as follows:
[0082] (1) The polystyrene microsphere dispersion is added to the polyethyleneimine solution under stirring, after stirring for 30 minutes, after washing with deionized water, the modified polystyrene microspheres are obtained;
[0083] Wherein, the concentration of the polystyrene microsphere dispersion is 80mg / mL, and the number of parts is 2.5mL, the concentration of the polyethyleneimine solution is 0.6wt%, and the number of parts is 10mL, the modified polystyrene prepared above The microspheres were redispersed in 25 mL of water to obtain a modified polystyrene microsphere dispersion with a mass concentration of 8 mg / mL.
[0084] (2) Add 100 μ...
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