Preparation method of vulcanized glyceryl trioleate and stainless steel tube drawing oil containing vulcanized glyceryl trioleate
A technology of triolein and stainless steel pipes, which is applied in the preparation of organic compounds, carboxylic acid esters, hydrogenated polysulfides/polysulfides, etc., can solve the problem of low surface quality of workpieces, high temperature, and mold High temperature and other problems, to achieve the effect of improving anti-wear and anti-rust performance
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Embodiment 1
[0020] Embodiment 1 (preparation of sulfurized glycerol trioleate)
[0021] The first step: the synthesis of glycerol trioleate, first add an appropriate amount of glycerin into a 250ml four-necked flask, gradually raise the temperature to 100°C, then add an appropriate amount of oleic acid in batches, fill with N 2 As a protective gas, toluene is used as water-carrying agent, toluenesulfonic acid is used as catalyst, stirring is started, and then the temperature is gradually raised to 130°C, and the reaction is carried out at this temperature for 7 hours, and the heating is stopped when no more water evaporates. After cooling and discharging, a light yellow oily triglyceride liquid was obtained.
[0022] The second step: the synthesis of sulfurized glycerol trioleate, dissolve the weighed sulfur in an appropriate amount of toluene, then add the glycerol trioleate obtained in the first step in a 250ml four-necked flask, start stirring, and fill with N 2 As a protective gas, ...
Embodiment 2
[0023] Example 2 (stainless steel pipe pulling oil containing sulfurized trioleate)
[0024] At room temperature, mix 24.8 parts of 500N base oil and 35 parts of 150BS base oil, turn on the stirring, heat with heat conduction oil, control the temperature at about 50°C, add 10 parts of high alkali value calcium sulfonate, stir for 20 minutes; then add 15 parts The sulfurized glycerol trioleate obtained in Example 1, 10 parts of dialkyl pentasulfide, 5 parts of dialkyl ammonium thiophosphate, 0.2 part of antioxidant; That is, the stainless steel pipe pulling oil product is obtained.
Embodiment 3
[0026] At room temperature, mix 24.8 parts of 500N base oil and 35 parts of 150BS base oil, turn on the stirring, heat with heat transfer oil, control the temperature at about 50°C, add 5 parts of high alkali value calcium sulfonate, stir for 20 minutes; then add 20 parts The sulfurized glycerol trioleate obtained in Example 1, 15 parts of dialkyl pentasulfides, 5 parts of dialkyl ammonium thiophosphate, and 0.2 part of antioxidant; That is, the stainless steel pipe pulling oil product is obtained.
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