Nano-silica particle packed bed super thermal insulation material and preparation method thereof

A technology of nano-silica and particle accumulation, applied in ceramic products, other household appliances, applications, etc., can solve the problems of insignificant improvement of mechanical properties of thermal insulation materials and increase of material costs, achieve strong mechanical properties and reduce air convection Thermal, environmentally friendly effect

Active Publication Date: 2018-04-06
CHINA UNIV OF MINING & TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

In this invention, the high temperature resistance and mechanical properties of silica airgel are improved by adding infrared opacifying agent and reinforcing fiber to silica airgel. Although the processing technology is simple, the added reinforcing fiber increases The cost of the material is reduced, and the mechanical properties of the prepared thermal insulation material are not significantly improved

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0021] A method for preparing a nano-silica particle packed bed super heat-insulating material, comprising the following steps:

[0022] (1) Under room temperature conditions, the nano-silica particles A with a particle diameter of 10nm and the nano-silica particles B with a particle diameter of 50nm are put into a ball mill with a mass ratio of 5:5, and the ball mill is first Ball milling at a speed of 200r / min for 60min, then ball milling at a speed of 100r / min for 60min, and mix uniformly to obtain nano-silica mixed particles A;

[0023] (2) Transfer nano-silica mixed particles A to an ultrasonic disperser, then add an infrared shielding agent to the ultrasonic disperser for ultrasonic dispersion for 50 minutes to obtain nano-silica mixed particles B, and the infrared shielding agent and nano-dioxide The mass ratio of silicon mixed particles A is 1:10; the infrared shielding agent is a mixture of potassium titanate whiskers and SiC nanoparticles, and the mass ratio of potas...

Embodiment 2

[0027] A method for preparing a nano-silica particle packed bed super heat-insulating material, comprising the following steps:

[0028] (1) Under room temperature conditions, the nano-silica particles A with a particle diameter of 25nm and the nano-silica particles B with a particle diameter of 75nm are put into a ball mill with a mass ratio of 7:3, and the ball mill is first Ball milling at a speed of 200r / min for 60min, then ball milling at a speed of 100r / min for 60min, and mix uniformly to obtain nano-silica mixed particles A;

[0029] (2) Transfer the nano-silica mixed particles A to an ultrasonic disperser, then add an infrared shielding agent to the ultrasonic disperser for ultrasonic dispersion for 60 minutes to obtain a nano-silica mixed particle B, and the infrared shielding agent and nano-dioxide The mass ratio of silicon mixed particles A is 1:10; the infrared shielding agent is a mixture of potassium titanate whiskers and SiC nanoparticles, and the mass ratio of ...

Embodiment 3

[0033]A method for preparing a nano-silica particle packed bed super heat-insulating material, comprising the following steps:

[0034] (1) Under room temperature conditions, the nano-silica particles A with a particle diameter of 40nm and the nano-silica particles B with a particle diameter of 100nm are put into a ball mill with a mass ratio of 8:2, and the ball mill is first Ball milling at a speed of 200r / min for 60min, then ball milling at a speed of 100r / min for 60min, and mix uniformly to obtain nano-silica mixed particles A;

[0035] (2) Transfer the nano-silica mixed particles A to an ultrasonic disperser, then add an infrared shielding agent to the ultrasonic disperser for ultrasonic dispersion for 70 minutes to obtain a nano-silica mixed particle B, and the infrared shielding agent and nano-dioxide The mass ratio of silicon mixed particles A is 1:8; the infrared shielding agent is a mixture of potassium titanate whiskers and SiC nanoparticles, and the mass ratio of p...

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Abstract

The invention discloses a nano-silica particle packed bed super thermal insulation material and a preparation method thereof. The method comprises the steps as follows: nano-silica particles A with the particle size of 10-40 nm and nano-silica particles B with the particle size of 50-100 nm are placed in a ball mill in the mass ratio being (5:5)-(8:2) at the room temperature, nano-silica mixed particles A are obtained after uniform mixing and then transferred to an ultrasonic dispersion machine, an infrared shielding agent is added to the ultrasonic dispersion machine for ultrasonic dispersionfor 50-70 min, and nano-silica mixed particles B are obtained, wherein the mass ratio of the infrared shielding agent to the nano-silica mixed particles A is (1:10)-(1:4); the nano-silica mixed particles B are pressed at the room temperature and the nano-silica particle packed bed super thermal insulation material is obtained. The production process can be simplified, the production cost can be reduced and the environmental pollution can be reduced on the basis that the prepared material has high-temperature resistance and excellent mechanical performance.

Description

technical field [0001] The invention belongs to the technical field of inorganic non-metallic materials, and specifically relates to a silicon dioxide thermal insulation material and a preparation method thereof, in particular to a nano-silica particle stacked bed super thermal insulation material and a preparation method thereof. Background technique [0002] Nanoporous super thermal insulation material refers to the thermal insulation material whose thermal conductivity is lower than that of "no convection air". Thermal insulation materials can be widely used in aerospace, national defense, chemical industry, metallurgy, electric power, construction and other fields. [0003] At present, nanoporous super thermal insulation materials are roughly divided into the following categories: nano-xonotlite, calcium silicate-based composite materials, nanofiber thermal insulation materials and silica airgel composite materials, among which silica airgel is The most widely studied t...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C04B38/00C04B30/02
CPCC04B30/02C04B2201/20C04B2201/32C04B2201/50C04B14/062C04B14/324C04B22/08C04B38/0074C04B38/0067C04B38/0054
Inventor 黄丛亮蔺子甄甄文开黄尊
Owner CHINA UNIV OF MINING & TECH
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